Specimen Handling, Preparation, and Treatments in Surface Characterization

Specimen Handling, Preparation, and Treatments in Surface Characterization
Author: Alvin W. Czanderna
Publisher: Springer Science & Business Media
Total Pages: 316
Release: 2006-04-11
Genre: Science
ISBN: 0306469138

With the development in the 1960s of ultrahigh vacuum equipment and techniques and electron, X-ray, and ion beam techniques to determine the structure and composition of interfaces, activities in the field of surface science grew nearly exponentially. Today surface science impacts all major fields of study from physical to biological sciences, from physics to chemistry, and all engineering disciplines. The materials and phenomena characterized by surface science range from se- conductors, where the impact of surface science has been critical to progress, to metals and ceramics, where selected contributions have been important, to bio- terials, where contributions are just beginning to impact the field, to textiles, where the impact has been marginal. With such a range of fields and applications, questions about sample selection, preparation, treatment, and handling are difficult to cover completely in one review article or one chapter. Therefore, the editors of this book have assembled a range of experts with experience in the major fields impacted by surface characterization. It is the only book which treats the subject of sample handling, preparation, and treatment for surface characterization. It is full of tricks, cautions, and handy tips to make the laboratory scientist’s life easier. With respect to organization of the book, the topics range from discussion of vacuum to discussion of biological, organic, elemental or compound samples, to samples prepared ex situ or in situ to the vacuum, to deposition ofthin films. Generic considerations of sample preparation are also given.

Handbook of Surface and Interface Analysis

Handbook of Surface and Interface Analysis
Author: John C. Riviere
Publisher: CRC Press
Total Pages: 671
Release: 2009-06-24
Genre: Science
ISBN: 1420007807

The original Handbook of Surface and Interface Analysis: Methods for Problem-Solving was based on the authors' firm belief that characterization and analysis of surfaces should be conducted in the context of problem solving and not be based on the capabilities of any individual technique. Now, a decade later, trends in science and technology appear

Scanning Auger Electron Microscopy

Scanning Auger Electron Microscopy
Author: Martin Prutton
Publisher: John Wiley & Sons
Total Pages: 384
Release: 2006-05-01
Genre: Technology & Engineering
ISBN: 0470866780

This eagerly-awaited volume has been edited by two academic researchers with extensive and reputable experience in this field. Emphasis is given to the underlying science of the method of Auger microscopy, and its instrumental realization, the visualization and interpretation of the data in the sets of the images that form the output of the measurements and the methods used to quantify the images. Imaging artefacts in Auger microscopy and methods to correct them are also detailed. The authors describe the technique of Multi-Spectral Auger Microscopy (MULSAM) and demonstrate its advantages in mapping complex multi-component surfaces. The book concludes with an outlook for the future of Auger microscopy.

Beam Effects, Surface Topography, and Depth Profiling in Surface Analysis

Beam Effects, Surface Topography, and Depth Profiling in Surface Analysis
Author: Alvin W. Czanderna
Publisher: Springer Science & Business Media
Total Pages: 447
Release: 2006-04-11
Genre: Technology & Engineering
ISBN: 0306469146

Many books are available that detail the basic principles of the different methods of surface characterization. On the other hand, the scientific literature provides a resource of how individual pieces of research are conducted by particular labo- tories. Between these two extremes the literature is thin but it is here that the present volume comfortably sits. Both the newcomer and the more mature scientist will find in these chapters a wealth of detail as well as advice and general guidance of the principal phenomena relevant to the study of real samples. In the analysis of samples, practical analysts have fairly simple models of how everything works. Superimposed on this ideal world is an understanding of how the parameters of the measurement method, the instrumentation, and the char- teristics of the sample distort this ideal world into something less precise, less controlled, and less understood. The guidance given in these chapters allows the scientist to understand how to obtain the most precise and understood measu- ments that are currently possible and, where there are inevitable problems, to have clear guidance as the extent of the problem and its likely behavior.

Auger Electron Spectroscopy

Auger Electron Spectroscopy
Author: John Wolstenholme
Publisher: Momentum Press
Total Pages: 217
Release: 2015-07-28
Genre: Technology & Engineering
ISBN: 160650682X

This book discusses the use of AES and SAM for the characterization of a wide range of technological materials. These include metals and alloys, semiconductors, nanostructures, and insulators. Its value as a tool for high-resolution elemental imaging and compositional depth profiling is illustrated. The application of the technique for obtaining compositional information from the surfaces, interfaces, and thin film structures of technological and engineering materials is demonstrated. This volume also describes the basic physical principles of AES in simple, largely qualitative, terms understandable by any undergraduate science or engineering student. Major components of typical Auger spectrometers are also described because an understanding of the instrumentation is important to anyone wishing to become a skilled analyst. Mention is also made of other types of analysis for which an Auger electron spectrometer may be used, for example, secondary electron microscopy, backscattered electron imaging, X-ray spectroscopy. The relationship between AES and other analysis techniques is also discussed.

Surface Modification of Textiles

Surface Modification of Textiles
Author: Q Wei
Publisher: Elsevier
Total Pages: 358
Release: 2009-08-26
Genre: Technology & Engineering
ISBN: 1845696689

The surface of textiles offers an important platform for functional modifications in order to meet special requirements for a variety of applications. The surface modification of textiles may be achieved by various techniques ranging from traditional solution treatment to biological approaches. This book reviews fundamental issues relating to textile surfaces and their characterisation and explores the exciting opportunities for surface modification of a range of different textiles.Introductory chapters review some important surface modification techniques employed for improved functional behaviour of textiles and the various surface characterisation methods available. Further chapters examine the different types of surface modification suitable for textiles, ranging from the use of plasma treatments and physical vapour deposition to the use of nanoparticles. Concluding chapters discuss surface modification strategies for various applications of textiles.Surface modification of textiles is a valuable resource for chemists, surface scientists, textile technologists, fibre scientists, textile engineers and textile students. - Reviews fundamental issues relating to textiles surfaces and their characterisation - Examines various types of surface modification suitable for textiles, including plasma treatments and nanoparticles - Discusses surface modification strategies for textile applications such as expansion into technical textile applications

Optimal Control Of Singularly Perturbed Linear Systems And Applications

Optimal Control Of Singularly Perturbed Linear Systems And Applications
Author: Zoran Gajic
Publisher: CRC Press
Total Pages: 334
Release: 2001-01-04
Genre: Technology & Engineering
ISBN: 9780203907900

Highlights the Hamiltonian approach to singularly perturbed linear optimal control systems. Develops parallel algorithms in independent slow and fast time scales for solving various optimal linear control and filtering problems in standard and nonstandard singularly perturbed systems, continuous- and discrete-time, deterministic and stochastic, mul

Catalysis with Supported Size-selected Pt Clusters

Catalysis with Supported Size-selected Pt Clusters
Author: Florian Frank Schweinberger
Publisher: Springer Science & Business Media
Total Pages: 231
Release: 2013-11-01
Genre: Science
ISBN: 3319014994

In his thesis, Florian Schweinberger investigates the influence of the precise size of catalytically active species on reactivity. In order to do this he carries out studies both in UHV and under ambient conditions for supported, size-selected Platium clusters (8-68 atoms). Schweinberger probed the electronic structure, adsorption properties and reactivity of two olefins on surfaces and Pt clusters in the submonolayer range. With adsorbed trichloroethene (TCE) a possible cluster-adsorbate induced change in the electronic structure, and for ethene a low-temperature, size-dependent self-/hydrogenation was observed.In a collaborative approach, Schweinberger and colleagues investigated Pt clusters under ambient pressure conditions. They characterised the clusters at at the local and integral level and tested for temperature stability. Experiments in gas phase ?-reactors and in liquid, as part of a hybrid photocatalytic system, revealed size-dependent reactivity.Overall this thesis is not only of interest for those who want to perform similar experiments but also provides superb scientific insights for researchers in the field.

Handbook of Nanofabrication

Handbook of Nanofabrication
Author:
Publisher: Academic Press
Total Pages: 307
Release: 2010-05-25
Genre: Technology & Engineering
ISBN: 0123751772

Many of the devices and systems used in modern industry are becoming progressively smaller and have reached the nanoscale domain. Nanofabrication aims at building nanoscale structures, which can act as components, devices, or systems, in large quantities at potentially low cost. Nanofabrication is vital to all nanotechnology fields, especially for the realization of nanotechnology that involves the traditional areas across engineering and science. - Includes chapters covering the most important Nanofabrication techniques, which aids comprehensive understanding of the latest manufacturing technologies encountered in the field of nano-level manufacturing which is essential for preparing for advanced study and application in nanofabrication techniques by enabling thorough understanding of the entire nanofabrication process as it applies to advanced electronic and related manufacturing technologies - Each chapter covers a nanofabrication technique comprehensively, which allows the reader to learn to produce nanometer-level products as well as collect, process, and analyze data, improve process parameters, and how to assist engineers in research, development and manufacture of the same - Includes contributions from recognized experts from around the globe, making the reader aware of variations in similar techniques applied in different geographical locations and is better positioned to establish all possible global applications

Comprehensive Nanoscience and Technology

Comprehensive Nanoscience and Technology
Author:
Publisher: Academic Press
Total Pages: 2785
Release: 2010-10-29
Genre: Science
ISBN: 0123743966

From the Introduction: Nanotechnology and its underpinning sciences are progressing with unprecedented rapidity. With technical advances in a variety of nanoscale fabrication and manipulation technologies, the whole topical area is maturing into a vibrant field that is generating new scientific research and a burgeoning range of commercial applications, with an annual market already at the trillion dollar threshold. The means of fabricating and controlling matter on the nanoscale afford striking and unprecedented opportunities to exploit a variety of exotic phenomena such as quantum, nanophotonic and nanoelectromechanical effects. Moreover, researchers are elucidating new perspectives on the electronic and optical properties of matter because of the way that nanoscale materials bridge the disparate theories describing molecules and bulk matter. Surface phenomena also gain a greatly increased significance; even the well-known link between chemical reactivity and surface-to-volume ratio becomes a major determinant of physical properties, when it operates over nanoscale dimensions. Against this background, this comprehensive work is designed to address the need for a dynamic, authoritative and readily accessible source of information, capturing the full breadth of the subject. Its six volumes, covering a broad spectrum of disciplines including material sciences, chemistry, physics and life sciences, have been written and edited by an outstanding team of international experts. Addressing an extensive, cross-disciplinary audience, each chapter aims to cover key developments in a scholarly, readable and critical style, providing an indispensible first point of entry to the literature for scientists and technologists from interdisciplinary fields. The work focuses on the major classes of nanomaterials in terms of their synthesis, structure and applications, reviewing nanomaterials and their respective technologies in well-structured and comprehensive articles with extensive cross-references. It has been a constant surprise and delight to have found, amongst the rapidly escalating number who work in nanoscience and technology, so many highly esteemed authors willing to contribute. Sharing our anticipation of a major addition to the literature, they have also captured the excitement of the field itself in each carefully crafted chapter. Along with our painstaking and meticulous volume editors, full credit for the success of this enterprise must go to these individuals, together with our thanks for (largely) adhering to the given deadlines. Lastly, we record our sincere thanks and appreciation for the skills and professionalism of the numerous Elsevier staff who have been involved in this project, notably Fiona Geraghty, Megan Palmer and Greg Harris, and especially Donna De Weerd-Wilson who has steered it through from its inception. We have greatly enjoyed working with them all, as we have with each other.