Sample Preparation of Soil and Plant Material for Isotope Ratio Mass Spectrometry

Sample Preparation of Soil and Plant Material for Isotope Ratio Mass Spectrometry
Author: International Atomic Energy Agency
Publisher:
Total Pages: 48
Release: 2019-07-02
Genre: Technology & Engineering
ISBN: 9789201020192

Stable isotope techniques can help improve soil management and crop nutrition. To ensure the quality of stable isotope analysis through isotope ratio mass spectrometry (IRMS), appropriate sample preparation is crucial. This publication presents methods for proper plant and soil sample processing for IRMS analysis. The information on such methods is often described in a summarized and non-comprehensive way without illustration of every step. This publication fills this gap and presents a selection of standard operating procedures and provides highly detailed guidance on sample preparation that will support practitioners in conducting reliable isotope analysis on plant and soil materials.

Mass Spectrometry of Soils

Mass Spectrometry of Soils
Author: Thomas Boutton
Publisher: CRC Press
Total Pages: 544
Release: 1996-05-30
Genre: Technology & Engineering
ISBN: 9780824796990

This work provides detailed coverage of the applications of proven spectometric techniques in soil science. It presents analytical approaches important in the study of pool sizes and the dynamics of macro- and micronutrients, the structure and function of soil organic matter, and the co-evolution of soils, plant communities and climate. Interdisciplinary perspectives from soil science, ecology, geology, chemistry, biogeochemistry, agronomy and physics, are offered.

Soil Sampling and Methods of Analysis

Soil Sampling and Methods of Analysis
Author: M.R. Carter
Publisher: CRC Press
Total Pages: 1264
Release: 2007-08-03
Genre: Science
ISBN: 1420005278

Thoroughly updated and revised, this second edition of the bestselling Soil Sampling and Methods of Analysis presents several new chapters in the areas of biological and physical analysis and soil sampling. Reflecting the burgeoning interest in soil ecology, new contributions describe the growing number and assortment of new microbiological

Sector Field Mass Spectrometry for Elemental and Isotopic Analysis

Sector Field Mass Spectrometry for Elemental and Isotopic Analysis
Author: Thomas Prohaska
Publisher: Royal Society of Chemistry
Total Pages: 667
Release: 2014-11-21
Genre: Science
ISBN: 1849735409

This book was triggered by the success story of sector field mass spectrometry in elemental and isotopic analysis from the early days when the first mass spectrum of Ne was presented a hundred years ago. The outstanding and unique features of sector field mass spectrometry - high sensitivity, high mass resolution and simultaneous multiple ion detection - paved the way for its successful and increasing application in different fields of science. Written, compiled and edited by worldwide renowned experts with profound expertise in sector field mass spectrometry related to elemental and isotopic analysis, this book is intended to provide deep insight into the topic along with fundamental knowledge about elemental and isotopic analysis. Aimed at scientists in the field of natural and life sciences, instrument manufacturers, practitioners and graduate students, this book provides solid information about the methodological background and analytical capabilities of sector field mass spectrometry. A detailed description of peculiarities and an overview of the most relevant applications making use of specific techniques using sector field mass analysers (ICP-MS, GDMS, TIMS, SIMS and IRMS) are given, including a presentation of the currently available commercial instruments. This approach guarantees that readers are thoroughly introduced to and familiarized with the fascinating inter- and transdisciplinary field of sector field mass spectrometry.

Modern Isotope Ratio Mass Spectrometry

Modern Isotope Ratio Mass Spectrometry
Author: I. T. Platzner
Publisher: John Wiley & Sons
Total Pages: 544
Release: 1997-10-22
Genre: Science
ISBN:

I. T. Platzner Atomic Energy Commission, Israel Including contributions from instrument manufacturers! Geological aging, chemical reaction mechanism studies, determination of atomic weights and investigation of metabolic pathways-these are all examples of the truly diverse nature of isotope ratio mass spectrometry (IRMS). With applications in fields as far apart as analytical chemistry and astronomy, geochemistry and biomedical science, it is little wonder that this technique is becoming increasingly popular. In Modern Isotope Ratio Mass Spectrometry,the first comprehensive book written on the subject for twenty-five years, examples from all these areas, and many more,are given. All modern developments in this fascinating field are discussed with special attention paid to technical details and instrumentation. Features of the book include: * comprehensive element-by-element review including 94 elements * applications chapter which stresses multi-disciplinary nature of subject * instrumentation chapter with contributions from three leading industrialists on state-of-the-art instrumentation

Encyclopedia of Analytical Science

Encyclopedia of Analytical Science
Author:
Publisher: Elsevier
Total Pages: 5142
Release: 2019-04-02
Genre: Science
ISBN: 008101984X

The third edition of the Encyclopedia of Analytical Science, Ten Volume Set is a definitive collection of articles covering the latest technologies in application areas such as medicine, environmental science, food science and geology. Meticulously organized, clearly written and fully interdisciplinary, the Encyclopedia of Analytical Science, Ten Volume Set provides foundational knowledge across the scope of modern analytical chemistry, linking fundamental topics with the latest methodologies. Articles will cover three broad areas: analytical techniques (e.g., mass spectrometry, liquid chromatography, atomic spectrometry); areas of application (e.g., forensic, environmental and clinical); and analytes (e.g., arsenic, nucleic acids and polycyclic aromatic hydrocarbons), providing a one-stop resource for analytical scientists. Offers readers a one-stop resource with access to information across the entire scope of modern analytical science Presents articles split into three broad areas: analytical techniques, areas of application and and analytes, creating an ideal resource for students, researchers and professionals Provides concise and accessible information that is ideal for non-specialists and readers from undergraduate levels and higher

Compound-specific Stable Isotope Analysis

Compound-specific Stable Isotope Analysis
Author: Maik A Jochmann
Publisher: Royal Society of Chemistry
Total Pages: 306
Release: 2015-11-09
Genre: Science
ISBN: 1782626107

The use of Compound-specific Stable Isotope Analysis (CSIA) is increasing in many areas of science and technology for source allocation, authentication, and characterization of transformation reactions. Until now, there have been no textbooks available for students with an analytical chemical background or basic introductory books emphasising the instrumentation and theory. This book is the first to focus solely on stable isotope analysis of individual compounds in sometimes complex mixtures. It acts as both a lecture companion for students and a consultant for advanced scientists in fields including forensic and environmental science. The book starts with a brief history of the field before going on to explain stable isotopes from scratch. The different ways to express isotope abundances are introduced together with isotope effects and isotopic fractionation. A detailed account of the required technical equipment and general procedures for CSIA is provided. This includes sections on derivatization and the use of microextraction techniques in GC-IRMS. The very important topic of referencing and calibration in CSIA is clearly described. This differs from approaches used in quantitative analysis and is often difficult for the newcomer to comprehend. Examples of successful applications of CSIA in food authenticity, forensics, archaeology, doping control, environmental science, and extraterrestrial materials are included. Applications in isotope data treatment and presentation are also discussed and emphasis is placed on the general conclusions that can be drawn from the uses of CSIA. Further instrumental developments in the field are highlighted and selected experiments are introduced that may act as a basis for a short practical course at graduate level.

Encyclopedia of Geoarchaeology

Encyclopedia of Geoarchaeology
Author: Allan S. Gilbert
Publisher: Springer
Total Pages: 0
Release: 2016-08-15
Genre: Social Science
ISBN: 9789400748279

Geoarchaeology is the archaeological subfield that focuses on archaeological information retrieval and problem solving utilizing the methods of geological investigation. Archaeological recovery and analysis are already geoarchaeological in the most fundamental sense because buried remains are contained within and removed from an essentially geological context. Yet geoarchaeological research goes beyond this simple relationship and attempts to build collaborative links between specialists in archaeology and the earth sciences to produce new knowledge about past human behavior using the technical information and methods of the geosciences. The principal goals of geoarchaeology lie in understanding the relationships between humans and their environment. These goals include (1) how cultures adjust to their ecosystem through time, (2) what earth science factors were related to the evolutionary emergence of humankind, and (3) which methodological tools involving analysis of sediments and landforms, documentation and explanation of change in buried materials, and measurement of time will allow access to new aspects of the past. This encyclopedia defines terms, introduces problems, describes techniques, and discusses theory and strategy, all in a format designed to make specialized details accessible to the public as well as practitioners. It covers subjects in environmental archaeology, dating, materials analysis, and paleoecology, all of which represent different sources of specialist knowledge that must be shared in order to reconstruct, analyze, and explain the record of the human past. It will not specifically cover sites, civilizations, and ancient cultures, etc., that are better described in other encyclopedias of world archaeology. The Editor Allan S. Gilbert is Professor of Anthropology at Fordham University in the Bronx, New York. He holds a B.A. from Rutgers University, and his M.A., M.Phil., and Ph.D. were earned at Columbia University. His areas of research interest include the Near East (late prehistory and early historic periods) as well as the Middle Atlantic region of the U.S. (historical archaeology). His specializations are in archaeozoology of the Near East and geoarchaeology, especially mineralogy and compositional analysis of pottery and building materials. Publications have covered a range of subjects, including ancient pastoralism, faunal quantification, skeletal microanatomy, brick geochemistry, and two co-edited volumes on the marine geology and geoarchaeology of the Black Sea basin.

Isotope Ratio Mass Spectrometry of Light Gas-Forming Elements

Isotope Ratio Mass Spectrometry of Light Gas-Forming Elements
Author: V.S. Sevastyanov
Publisher: CRC Press
Total Pages: 244
Release: 2016-04-19
Genre: Science
ISBN: 146659408X

Isotope Ratio Mass Spectrometry of Light Gas-Forming Elements explores different methods of isotope analysis, including spark, secondary ion, laser, glow discharge, and isotope ratio mass spectrometry. It explains how to evaluate the isotopic composition of light elements (H, C, N, O) in solid, liquid, and gaseous samples of organic and inorganic s

Carbon Isotope Techniques

Carbon Isotope Techniques
Author: David C. Coleman
Publisher: Academic Press
Total Pages: 287
Release: 2012-12-02
Genre: Science
ISBN: 032315767X

Carbon Isotope Techniques deals with the use of carbon isotopes in studies of plant, soil, and aquatic biology. Topics covered include photosynthesis/translocation studies in terrestrial ecosystems; carbon relationships of plant-microbial symbioses; microbe/plant/soil interactions; and environmental and aquatic toxicology. Stable carbon isotope ratios of natural materials are also considered. Comprised of 15 chapters, this book begins with an introduction to radiation-counting instruments used in measuring the radioactivity in soil and plant samples containing carbon-14. The discussion then turns to the basic methods of 14C use in plant science, highlighted by three examples of applications in the field of plant physiology and ecology. Subsequent chapters explore the use of carbon isotope techniques for analyzing the carbon relationships of plant-microbial symbioses; the interactions of microbes, plants, and soils; and the degradation of herbicides and organic xenobiotics. Carbon dating and bomb carbon are also described. The final section is devoted to the uses and procedures for 13C and 11C. This monograph is intended for advanced undergraduate or graduate students, as well as generalist scientists who have not previously used radioisotopes or stable isotopes in their research.