Preparative Methods In Solid State Chemistry
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| Author | : Paul Hagenmuller |
| Publisher | : Elsevier |
| Total Pages | : 621 |
| Release | : 2012-12-02 |
| Genre | : Science |
| ISBN | : 0323144365 |
Preparative Methods in Solid State Chemistry deals with the preparative methods used in solid state chemistry and highlights the importance of the chemist's role in preparing materials of desired quality as well as obtaining materials according to the requirements of the user such as the physicist. Topics covered range from high-pressure techniques in preparative chemistry to methods of growing single crystals of high-melting-point oxides. This book is comprised of 14 chapters and begins with an overview of possibilities for high-pressure synthesis, as well as the methods used to obtain high pressures, including transmission by gaseous or liquid fluids or in the solid state. The method of shock waves is then considered both from the point of view of thermodynamics and thermoelasticity, along with the possibility of using superpressures for evidently revolutionary applications. Subsequent chapters focus on the synthesis of single crystals of refractory oxides either at high temperatures (essentially liquid-solid transformations) or at lower temperatures in the presence of a solvent or a chemical reagent. The production of single crystals by electrolytic reduction in molten salts is also described. Numerous examples of vapor transport reactions in a temperature gradient are presented. This monograph should be of interest to chemists and students of solid state chemistry.
| Author | : Lesley Smart |
| Publisher | : Springer |
| Total Pages | : 408 |
| Release | : 1995 |
| Genre | : Science |
| ISBN | : |
| Author | : Aaron Wold |
| Publisher | : Springer Science & Business Media |
| Total Pages | : 250 |
| Release | : 2012-12-06 |
| Genre | : Science |
| ISBN | : 9401114765 |
The subject matterofsolid state chemistry lies within the spheres ofboth physical and inorganic chemistry. In addition, there is a large overlap with solid state physics and materials engineering. However, solid state chemistry has still to be recognized by the general body ofchemists as a legitimate subfield ofchemistry. The discipline is not even well defined as to content and has many facets that make writing a textbook a formidable task. The early studies carried out in the United States by Roland Ward and his co workers emphasized the synthesisofnew materials and the determination oftheir structure. His work on doped alkaline earth sulfides formed the basis for the development of infrared phosphors and his pioneering studies on oxides were important in understanding the structural features of both the perovskite oxides as well as the magnetoplumbites. In 1945, A. F. Wells published the first edition of Structural Inorganic Chemistry. This work attempts to demonstrate that the synthesis, structure, and properties of solids form an important part of inorganic chemistry. Now, after almost 50 years during which many notable advances have been made in solid state chemistry, it is still evident that the synthesis, structure determination, and properties of solids receive little attention in most treatments of inorganic chemistry. The development of the field since the early studies of Roland Ward (early 1940s) has been rapid.
| Author | : Lesley E. Smart |
| Publisher | : CRC Press |
| Total Pages | : 483 |
| Release | : 2016-04-19 |
| Genre | : Science |
| ISBN | : 1439847924 |
Building a foundation with a thorough description of crystalline structures, Solid State Chemistry: An Introduction, Fourth Edition presents a wide range of the synthetic and physical techniques used to prepare and characterize solids. Going beyond basic science, the book explains and analyzes modern techniques and areas of research. The book covers: A range of synthetic and physical techniques used to prepare and characterize solids Bonding, superconductivity, and electrochemical, magnetic, optical, and conductive properties STEM, ionic conductivity, nanotubes and related structures such as graphene, metal organic frameworks, and FeAs superconductors Biological systems in synthesis, solid state modeling, and metamaterials This largely nonmathematical introduction to solid state chemistry includes basic crystallography and structure determination, as well as practical examples of applications and modern developments to offer students the opportunity to apply their knowledge in real-life situations and serve them well throughout their degree course. New in the Fourth Edition Coverage of multiferroics, graphene, and iron-based high temperature superconductors, the techniques available with synchrotron radiation, and metal organic frameworks (MOFs) More space devoted to electron microscopy and preparative methods New discussion of conducting polymers in the expanded section on carbon nanoscience
| Author | : Richard Dronskowski |
| Publisher | : John Wiley & Sons |
| Total Pages | : 3912 |
| Release | : 2017-10-23 |
| Genre | : Technology & Engineering |
| ISBN | : 3527325875 |
This most comprehensive and unrivaled compendium in the field provides an up-to-date account of the chemistry of solids, nanoparticles and hybrid materials. Following a valuable introductory chapter reviewing important synthesis techniques, the handbook presents a series of contributions by about 150 international leading experts -- the "Who's Who" of solid state science. Clearly structured, in six volumes it collates the knowledge available on solid state chemistry, starting from the synthesis, and modern methods of structure determination. Understanding and measuring the physical properties of bulk solids and the theoretical basis of modern computational treatments of solids are given ample space, as are such modern trends as nanoparticles, surface properties and heterogeneous catalysis. Emphasis is placed throughout not only on the design and structure of solids but also on practical applications of these novel materials in real chemical situations.
| Author | : M. D. Cohen |
| Publisher | : Elsevier |
| Total Pages | : 231 |
| Release | : 2013-10-22 |
| Genre | : Science |
| ISBN | : 1483284697 |
Organic Solid-State Chemistry–2 presents the solid state reactions in molecular crystals. This book discusses the correlations of the chemical structures of products from organic solid state reactions with the molecular packing in the reactant crystal structures. Organized into 10 chapters, this book begins with an overview of the molecular behavior after the chemical transition state. This text then examines the electron paramagnetic resonance methods, which offer many features in connection with the study of chemical reactions in which a paramagnetic species is a product or a reactant. Other chapters consider the interpretation of radiationless transitions, thermal reactions, and photochemical decompositions and rearrangements. The final chapter deals with the experimental results concerning electron and hole production in anthracene crystals, with emphasis on the relevance of these studies to the fundamental question of the nature of the excess electron states in these low mobility crystals. This book is a valuable resource for solid state chemists, photochemists, spectroscopists, scientists, and research workers.
| Author | : Riadh Marzouki |
| Publisher | : BoD – Books on Demand |
| Total Pages | : 138 |
| Release | : 2020-10-07 |
| Genre | : Technology & Engineering |
| ISBN | : 1838802231 |
New crystalline materials (organic, inorganic, hybrid) are promising for various applications, including electrical, piezoelectric, ferroelectric, magnetic, and catalytic processes. In addition, given their remarkable structural richness, these materials exhibit several interesting physical properties, such as ionic conduction, ion exchange, and others. Crystal growth, morphology, and grain size are factors influencing these physical properties. This book examines methods of synthesis of the most common crystalline materials and describes nucleation and crystal growth of various materials.
| Author | : Ashok Kumar Jha |
| Publisher | : CRC Press |
| Total Pages | : 291 |
| Release | : 2023-08-04 |
| Genre | : Technology & Engineering |
| ISBN | : 1000735664 |
Solid-state reactions have been growing in importance in the preparation of solids, crystal growth, and single crystals of elements. In this new volume, the author discusses in depth recent advances in solid-state chemistry, the latest techniques of characterization of solids, and several new dimensions of solid-state problems. Solid-state reactions, their kinetics, phase transitions, and magnetic properties are discussed in detail, along with electrical properties, semiconductors, metals, and insulators, with examples and explanations. Dielectric, piezoelectric, and ferroelectric properties of solids have been considered as well. Different theories of catalysis and adsorption isotherms are covered, and the author includes several experimental findings as well. And of course, preparation of new solids by taking advantage of recent experimental techniques have also been included in this volume. This volume provides a complete description of solid-state reactions, electrical conductivity, characterization of solids, organic solids, and intercalation between layers of solids. The band theories of metals, semiconductors, and insulators are covered. In characterization of solids, TGA, DTA, DSC, FTIR and PXRD techniques have been described. Preparation and properties of organic solids are also explained. Dielectric properties, photovoltaic effects, piezo electricity, ferroelectricity, and antiferroelectricity have been dealt with, giving relatable examples. A number of excitation energy levels giving rise to luminescence and photoluminescence have been explained under the topic optical processes. Diamagnetic, paramagnetic, and ferromagnetic behaviors of solids are also explained.
| Author | : Chintamani Nagesa Ramachandra Rao |
| Publisher | : Cambridge University Press |
| Total Pages | : 528 |
| Release | : 1986-11-06 |
| Genre | : Technology & Engineering |
| ISBN | : 9780521301923 |
This book presents the highlights of modern solid state chemistry, an emerging area of chemical science. In adopting a unified and up-to-date approach the authors take the reader to the very frontiers of the subject, which is concerned primarily with new methods of synthesis, identification and characterization of solids, and above all with new strategies for tailor-making materials with desirable and controllable properties. The eight chapters are devoted to structure, methods of characterization, preparative strategies, phase transitions, defects and non-stoichiometry, structure-property relations, materials design, and reactivity of solids. Each of these reflects the way solid state chemistry is growing today and brings out the flavour of the subject to show how it works. In addition, every chapter ends with a list of important references.
| Author | : C. N. R. Rao |
| Publisher | : Cambridge University Press |
| Total Pages | : 568 |
| Release | : 1997-02-28 |
| Genre | : Science |
| ISBN | : 9780521499071 |
In the new edition of this widely praised textbook, all the chapters have been revised and the authors have brought the work completely up to date by the addition of new material on numerous topics. In recent years, solid state chemistry has emerged as a very important element of mainstream chemistry and materials science. Students, teachers and researchers need to understand the chemistry of solids because of the crucial role this plays in determining the properties of materials. An understanding of solid state chemistry is also essential in materials design, and many fascinating relationships between the structure and properties of solids have been discovered by chemists. This text requires only an understanding of basic physics, chemistry and crystallography, and is enhanced with the most recent examples, case studies and references. It will be of value to advanced students and researchers studying solid state chemistry and materials science as a text and reference work.
