Newer Methods Of Preparative Organic Chemistry V2
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Author | : Wilhelm Foerst |
Publisher | : Elsevier |
Total Pages | : 434 |
Release | : 2012-12-02 |
Genre | : Science |
ISBN | : 032315042X |
Newer Methods of Preparative Organic Chemistry, Volume II focuses on several improved methods in preparative organic chemistry. This book presents a variety of detailed laboratory procedures in organic chemistry. Organized into 14 chapters, this volume starts with an overview of the compound acetoacetaldehyde, which is prepared from sodium formylacetone with acetic anhydride in ether. This text then explains the requirements I a rational peptide synthesis, including controlled reaction conditions, retention of optical activity, high yields, and analogous applicability to free amino acids and to terminal amino acids of oligopeptides. Other chapters consider the general equation of the inner anhydride of acetic acid. This book discusses as well the relation between polarity and reactivity in phosphines. The final chapter deals with the methylation of aromatic compounds, which is a typical radical reaction. This book is intended for synthetic organic chemists. Graduate students and research workers in the fields of organic chemistry and biochemistry will find this book useful.
Author | : Wilhelm Foerst |
Publisher | : Elsevier |
Total Pages | : 559 |
Release | : 2012-12-02 |
Genre | : Science |
ISBN | : 0323146104 |
Newer Methods of Preparative Organic Chemistry, Volume III focuses on the improved methods in preparative organic chemistry. This book presents a variety of topics, including the synthesis of acetylenes, methods for the preparation of pyrylium salts, and the use of phosphoric acid chlorides in the preparation of esters of phosphoric acids. Organized into 11 chapters, this volume starts with an overview of the reaction between methylene and sulfur involving dehydrogenation or oxidation. This text then examines the chemistry of pyridine, which exhibits different reaction characteristics than benzene. Other chapters consider the cyclic derivatives of carboxylic acids, such as lactams, lactones, or thiolactones, which can be converted by partial reduction into heterocycles of the same ring size. The final chapter outlines the fundamental reactions of diazoketones and discusses the preparative significance of the diazoketones. This book is a valuable resource for synthetic organic chemists involved in research institutions and industrial laboratories.
Author | : Alan Haines |
Publisher | : Elsevier |
Total Pages | : 488 |
Release | : 2012-12-02 |
Genre | : Science |
ISBN | : 0323148441 |
Methods for the Oxidation of Organic Compounds: Alcohols, Alcohol Derivatives, Alkyl Halides, Nitroalkanes, Alkyl Azides, Carbonyl Compounds, Hydroxyarenes and Aminoarenes describes the different methods used for the controlled oxidation of alcohols, alcohol derivatives, alkyl halides, nitroalkanes, alkyl azides, carbonyl compounds, hydroxyarenes, and aminoarenes. Most of the oxidative techniques considered are illustrated with detailed experimental procedures taken from the literature. This book is comprised of eight chapters and begins with a discussion on the oxidation of alcohols, with particular emphasis on the formation of carbonyl compounds and carboxylic acids. The following chapters focus on the oxidation of esters and alkyl halides; ethers, acetals, and metal derivatives of alcohols; amines, nitro compounds, and azides; carbonyl compounds; 1,2-diols and related compounds; and hydroxyarenes, aminoarenes, dihydroxyarenes, diaminoarenes, and aminohydroxyarenes. Methods such as catalytic oxidation, catalytic dehydrogenation, and electrochemical and biochemical oxidation are mentioned. This monograph should be of interest to organic chemists and research students.
Author | : William Sabel |
Publisher | : Elsevier |
Total Pages | : 207 |
Release | : 2013-09-03 |
Genre | : Science |
ISBN | : 1483213773 |
Basic Techniques of Preparative Organic Chemistry covers a detailed guide for carrying out the procedures commonly needed in preparative organic chemistry. The book discusses the nature of organic reactions; the basic principles of preparative organic chemistry; unit operations; and good laboratory practice. The text then provides a review of apparatus and equipment and describes the potential hazards involved in a chemical operation, such as toxicity, bodily injuries, smoking, fire, explosion, and implosion. Techniques and unit operations for carrying out a reaction and for isolating and purifying a reaction product; and the criteria for and methods of assessing purity are also considered. The book further tackles packing and storing products and samples and making reports and communications. Students taking organic chemistry courses will find the text useful.
Author | : Wilhelm Foerst |
Publisher | : |
Total Pages | : 0 |
Release | : 1971 |
Genre | : Organic compounds |
ISBN | : |
Author | : Norman Kharasch |
Publisher | : Elsevier |
Total Pages | : 357 |
Release | : 2013-10-22 |
Genre | : Reference |
ISBN | : 1483149374 |
Index to Reviews, Symposia Volumes and Monographs in Organic Chemistry for the Period 1940-1960 presents a resume of published monographs, reviews, and symposia lectures in organic chemistry. The editors adopted the plan of listings by symposia volume or journal, backed up by the total subject and author indexes. In this way the user can readily locate a particular article through the author index or the subject index; or should he recall that an article appeared in a particular source, the chronological listing in that source can be scanned quickly. The Index gives a convenient overview of the accomplishments of organic chemists during this very prolific period of the growth of the field. Frequently, several articles on the same or similar subject appear, hence the historical perspective can be sensed by rapid evaluation of the reviews selected. This Index will be useful to research workers, teachers and students. It will also assist editors and authors to select specific areas which require critical review.
Author | : Wilhelm Foerst |
Publisher | : |
Total Pages | : 684 |
Release | : 1948 |
Genre | : Chemistry, Organic |
ISBN | : |
Author | : J.H. Simons |
Publisher | : Elsevier |
Total Pages | : 577 |
Release | : 2012-12-02 |
Genre | : Science |
ISBN | : 0323145434 |
Fluorine Chemistry, Volume II focuses on studies on fluorocarbons and fluorocarbon derivatives. Composed of various literature, the book first discusses fluorine-containing complex salts and acids. The complex fluorides of alkali metals, beryllium, boron, carbon, silicon, germanium, tin, and lead are described. The text also looks at research on halogen fluorides. The physical properties of chlorine, bromine, and iodine fluorides; halogen fluorides as ionizing solvents; and acids and bases in iodine pentafluoride and chlorine trifluoride are discussed. The book discusses analytical chemistry of fluorine and fluorine-containing compounds. Analysis of gaseous samples; separation and isolation of fluorine; qualitative detection and identification of fluorine; and determination of fluorine in specific materials are described. The text also focuses on organic compounds containing fluorine. Alcohols, acids and their derivatives, polymer containing fluorines, amines, amino acids, drugs, dyes, and pesticides are discussed as well. The book further looks at metallic compounds containing fluorocarbon radicals and organometallic compounds containing fluorine, fluorocarbon chemistry, and the infrared spectra of fluorocarbons and related compounds. The text is a vital source of information for readers wanting to study fluorocarbons and fluorocarbon derivatives.
Author | : Alan Haines |
Publisher | : Elsevier |
Total Pages | : 409 |
Release | : 2012-12-02 |
Genre | : Science |
ISBN | : 0323151787 |
Methods for the Oxidation of Organic Compounds: Alkanes, Alkenes, Alkynes, and Arenes is an account of the different methods used for the controlled oxidation of alkanes, alkenes, alkynes, and arenes. Most of the oxidative techniques considered are illustrated with detailed experimental procedures taken from the literature. This book is comprised of five chapters and begins with a discussion on alkanes, alkyl groups, and hydrocarbon residues. The formation of alkenes, alcohols, hydroperoxides, dialkyl peroxides, cyclic peroxides, ethers, and esters as well as aldehydes, ketones, and carboxylic acids is described, together with the aromatization of cyclic systems. The following chapters are devoted to alkenes, alkynes, and arenes and focus on the formation of compounds ranging from 1,2-diols and oxiranes (1,2-epoxides) to 1,2-dicarbonyl compounds, phenols and their derivatives, and quinones. The formation of dialkynes by oxidative coupling of 1-alkynes is described, along with the oxidative cleavage of arenes and oxidative coupling of phenols. This monograph should be of interest to organic chemists and research students.
Author | : Jie Jack Li |
Publisher | : John Wiley & Sons |
Total Pages | : 704 |
Release | : 2011-09-28 |
Genre | : Science |
ISBN | : 1118092848 |
The up-to-DATE guide to name reactions in heterocyclic chemistry Name Reactions in Heterocyclic Chemistry II presents a comprehensive treatise on name reactions in heterocyclic chemistry, one of the most exciting and important fields within organic chemistry today. The book not only covers fresh ground, but also provides extensive information on new and/or expanded reactions in: Three- and four-membered heterocycles Five-membered heterocycles (pyrroles and pyrrolidines, indoles, furans, thiophenes, and oxazoles) Six-membered heterocycles, including pyridines, quinolines, and isoquinolines Featuring contributions from the leading authorities in heterocyclic chemistry. Each section includes a description of the given reaction, as well as the relevant historical perspective, mechanism, variations and improvements, synthetic utilities, experimental details, and references to the current primary literature. The reactions covered in Name Reactions in Heterocyclic Chemistry have been widely adopted in all areas of organic synthesis, from the medicinal/pharmaceutical field, to agriculture, to fine chemicals, and the book brings the most cutting-edge knowledge to practicing synthetic chemists and students, along with the tools needed to synthesize new and useful molecules.