Microwave-Assisted Sample Preparation for Trace Element Determination

Microwave-Assisted Sample Preparation for Trace Element Determination
Author: Erico Marlon Moraes Flores
Publisher: Newnes
Total Pages: 415
Release: 2014-05-03
Genre: Science
ISBN: 0444594442

Microwave-Assisted Sample Preparation for Trace Element Analysis describes the principles, equipment, and applications involved in sample preparation with microwaves for trace element analysis. The book covers well-established applications as well as new trends in this field. Hot topics such as sample preparation for speciation, metabolomics, and halogen determination, as well as the alternatives of sample preparation for special samples (for example, carbon nanotubes, polymers, petroleum products), are also discussed. The use of microwaves in sample preparation has increased in recent decades. Several applications of microwaves for sample preparation can be found in the literature for practically all types of sample matrices, especially for the determination of trace elements by atomic spectrometric techniques, safely and cleanly reducing the time involved in this step. Microwave-assisted sample preparation is not only a tool for research but also for routine analysis laboratories; the state-of-the-art in sample preparation in trace element analysis. This book is the only resource for chemists specifically focused on this topic. - The first book to describe the principles, equipment, and applications in microwave-assisted sample preparation - Written by experts in the field who provide a comprehensive overview of the important concepts - Introduces new alternatives and trends in microwave-assisted techniques

Sample Preparation for Trace Element Analysis

Sample Preparation for Trace Element Analysis
Author: Zoltan Mester
Publisher: Elsevier
Total Pages: 1339
Release: 2003-12-16
Genre: Science
ISBN: 0080545483

Following the collection of a sample, every analytical chemist will agree that its subsequent preservation and processing are of paramount importance. The availability of high performance analytical instrumentation has not diminished this need for careful selection of appropriate pretreatment methodologies, intelligently designed to synergistically elicit optimum function from these powerful measurement tools. Sample Preparation for Trace Element Analysis is a modern, comprehensive treatise, providing an account of the state-of-the art on the subject matter. The book has been conceived and designed to satisfy the varied needs of the practicing analytical chemist. It is a multi-author work, reflecting the diverse expertise arising from its highly qualified contributors. The first five chapters deal with general issues related to the determination of trace metals in varied matrices, such as sampling, contamination control, reference materials, calibration and detection techniques. The second part of the book deals with extraction and sampling technologies (totaling 15 chapters), providing theoretical and practical hints for the users on how to perform specific extractions. Subsequent chapters overview seven major representative matrices and the sample preparation involved in their characterization. This portion of the book is heavily based on the preceding chapters dealing with extraction technologies. The last ten chapters are dedicated to sample preparation for trace element speciation.- First title to provide comprehensive sample preparation information, dealing specifically with the analysis of samples for trace elements. - The 39 chapters are authored by international leaders of their fields.

ICP-MS and Trace Element Analysis as Tools for Better Understanding Medical Conditions

ICP-MS and Trace Element Analysis as Tools for Better Understanding Medical Conditions
Author:
Publisher: Elsevier
Total Pages: 200
Release: 2022-05-25
Genre: Science
ISBN: 0444643486

ICP-MS and Trace Element Analysis as Tools for Better Understanding Medical Conditions, Volume 97 discusses trace elements and how they play an important role in biological functions and metabolism in the human body. Chapters cover Biomedical analysis by ICP-MS: A focus on single cell, Advanced statistical tools and machine learning applied to trace element analysis associated with medical conditions, ICP-MS as a tool to understand trace element homeostasis in neurological disorders, High-precision isotopic analysis of essential mineral elements – possibilities for medical diagnosis and prognosis, Exploring ICP-MS as a versatile technique: From imaging to chemical speciation, and more. - Discusses the latest diagnosis/pathologies using ICP-MS analysis - Covers metals, isotopes and metalorganic species for medical conditions - Includes ICP-MS-based techniques

Microwave Chemistry

Microwave Chemistry
Author: Giancarlo Cravotto
Publisher: Walter de Gruyter GmbH & Co KG
Total Pages: 552
Release: 2017-09-25
Genre: Science
ISBN: 3110479931

Microwave Chemistry has changed the way to work in chemical laboratories and is an established state-of-the-art technology to accelarate and enhance chemical processes. This book not only gives an overview of the technology, its historical development and theoretical background, but also presents its exceptionally broad spectrum of applications. Microwave Chemistry enables graduate students and scientist to learn and apply its methods successfully.

Handbook of Trace Analysis

Handbook of Trace Analysis
Author: Irena Baranowska
Publisher: Springer
Total Pages: 458
Release: 2015-08-13
Genre: Science
ISBN: 3319196146

This handbook is unique in its comprehensive coverage of the subject and focus on practical applications in diverse fields. It includes methods for sample preparation, the role of certified reference materials, calibration methods and statistical evaluation of the results. Problems concerning inorganic and bioinorganic speciation analysis, as well as special aspects such as trace analysis of noble metals, radionuclides and volatile organic compounds are also discussed. A significant part of the content presents applications of methods and procedures in medicine (metabolomics and therapeutic drug monitoring); pharmacy (the analysis of contaminants in drugs); studies of environmental samples; food samples and forensic analytics – essential examples that will also facilitate problem solving in related areas.

Inorganic Trace Analytics

Inorganic Trace Analytics
Author: Henryk Matusiewicz
Publisher: Walter de Gruyter GmbH & Co KG
Total Pages: 460
Release: 2017-12-18
Genre: Science
ISBN: 3110366738

Highly accurate chemical speciation is of great importance in environmental, clinical, and food sciences, as well as in archaeometry. Trace analysis via atomic spectrometry, mass spectroscopy, gas chromatography, electron microprobing, or X-ray absorption spectroscopy provides detailed information on surface and sub-surface domain of samples. The book comprehensively presents modern techniques, timely application, and data modeling.

Encyclopedia of Analytical Science

Encyclopedia of Analytical Science
Author:
Publisher: Elsevier
Total Pages: 5142
Release: 2019-04-02
Genre: Science
ISBN: 008101984X

The third edition of the Encyclopedia of Analytical Science, Ten Volume Set is a definitive collection of articles covering the latest technologies in application areas such as medicine, environmental science, food science and geology. Meticulously organized, clearly written and fully interdisciplinary, the Encyclopedia of Analytical Science, Ten Volume Set provides foundational knowledge across the scope of modern analytical chemistry, linking fundamental topics with the latest methodologies. Articles will cover three broad areas: analytical techniques (e.g., mass spectrometry, liquid chromatography, atomic spectrometry); areas of application (e.g., forensic, environmental and clinical); and analytes (e.g., arsenic, nucleic acids and polycyclic aromatic hydrocarbons), providing a one-stop resource for analytical scientists. Offers readers a one-stop resource with access to information across the entire scope of modern analytical science Presents articles split into three broad areas: analytical techniques, areas of application and and analytes, creating an ideal resource for students, researchers and professionals Provides concise and accessible information that is ideal for non-specialists and readers from undergraduate levels and higher

Advances in Microwave Chemistry

Advances in Microwave Chemistry
Author: Bimal K Banik
Publisher: CRC Press
Total Pages: 415
Release: 2018-12-07
Genre: Science
ISBN: 1351240471

Advances in Microwave Chemistry discusses the novel bond formation methodologies, synergistic effects of microwaves with other entities, sample preparation including digestion, combustion, and extraction techniques, as well as selectivity in chemical processes. Recent updates are provided on microwave-assisted syntheses of pharmacologically significant aza-, oxo- and other heterocycles, including lactams, nucleosides, bile acids and sterols, the preparation of nanomaterials, composites, and absorber layer materials for thin film. This book also incorporates comparative discussions involving microwave irradiation with conventional methods in different aspects of organic, inorganic, medicinal, and green chemistry. Key Features: Provides a comparative discussion on microwave irradiation with conventional methods in different aspects of organic, inorganic, medicinal, and green chemistry Presents recent applications of microwave radiation in biocatalysis Offers a complete package correlating various aspects of microwaves in organic syntheses, the biological impact of products formed in reactions, pharmacological features, and environmental sustainability of the procedures Explains microwave-induced reactions on structurally complex bile acids and sterols Stands as a valuable and unique addition to the well-established book series, New Directions in Organic and Biological Chemistry

Trends in Sample Preparation

Trends in Sample Preparation
Author: Marco Aurélio Zezzi Arruda
Publisher: Nova Publishers
Total Pages: 318
Release: 2007
Genre: Science
ISBN: 9781600211188

Micro Sampling for Solid and Slurries Analytical Methods; Microwave-assisted Procedures for Sample Preparation: Recent Developments; Trends in Sample Preparation using Combustion Techniques; Sample Preparation of Atmospheric Aerosols for Elemental Analysis and Fractionation Studies; Extraction and Pre-Concentration Techniques for Chromatographic Analysis; Strategies in Sample Preparation for Applications in Analytical Electrochemistry In-Line Sample Preparation in Flow Analysis; The Role of Vanguard-Rearguard Strategies in Sample Preparation in Routine AnaIytical Laboratories; Strategies for Sample Preparation Focusing on Biomolecules Determination/Characterization.

Ion-Exchange Chromatography and Related Techniques

Ion-Exchange Chromatography and Related Techniques
Author: Pavel Nesterenko
Publisher: Elsevier
Total Pages: 646
Release: 2023-11-15
Genre: Technology & Engineering
ISBN: 0443153701

Ion-Exchange Chromatography and Related Techniques defines the current state-of-the-art in ion-exchange chromatography and related techniques and their implementation in laboratory and industrial practice. This book provides a compact source of information to facilitate the transfer of knowledge and experience acquired by separation science specialists to colleagues from diverse backgrounds who need to acquire fundamental and practical information to facilitate progress in research and management functions reliant on information acquired by separation. Individual chapters written by recognized experts lending credibility to the work will allow this book to serve as a high value reference source of current information for analytical and biopharmaceutical chemists. - Includes individual chapters written by recognized authoritative and visionary experts in the field to provide an overview and focused treatment of a single topic - Presents comprehensive coverage of ion-exchange techniques from theory, to methods, to selected applications for ions and biopolymers - Provides Tables and diagrams with commonly used data to facilitate practical work, comparison of results and decision-making