Industrial Crystallization of Melts

Industrial Crystallization of Melts
Author: C.M. Van 't Land
Publisher: CRC Press
Total Pages: 306
Release: 2004-09-24
Genre: Science
ISBN: 0203021134

At the interface of chemical industry operations, equipment manufacturer input, and the scientific literature, Industrial Crystallization of Melts explores and explains melt crystallization and purification in the industrial arena. This comprehensive account details the orderly conversion of melts into solid, salable end materials and procedures fo

Industrial Crystallization of Melts

Industrial Crystallization of Melts
Author: C.M. Van 't Land
Publisher: CRC Press
Total Pages: 393
Release: 2004-09-24
Genre: Science
ISBN: 1135571708

At the interface of chemical industry operations, equipment manufacturer input, and the scientific literature, Industrial Crystallization of Melts explores and explains melt crystallization and purification in the industrial arena. This comprehensive account details the orderly conversion of melts into solid, salable end materials and procedures fo

Handbook of Industrial Crystallization

Handbook of Industrial Crystallization
Author: Allan Myerson
Publisher: Butterworth-Heinemann
Total Pages: 329
Release: 2002-01-08
Genre: Technology & Engineering
ISBN: 0080533515

Crystallization is an important separation and purification process used in industries ranging from bulk commodity chemicals to specialty chemicals and pharmaceuticals. In recent years, a number of environmental applications have also come to rely on crystallization in waste treatment and recycling processes.The authors provide an introduction to the field of newcomers and a reference to those involved in the various aspects of industrial crystallization. It is a complete volume covering all aspects of industrial crystallization, including material related to both fundamentals and applications. This new edition presents detailed material on crystallization of biomolecules, precipitation, impurity-crystal interactions, solubility, and design.Provides an ideal introduction for industrial crystallization newcomers Serves as a worthwhile reference to anyone involved in the fieldCovers all aspects of industrial crystallization in a single, complete volume

Crystallization

Crystallization
Author: Wolfgang Beckmann
Publisher: John Wiley & Sons
Total Pages: 370
Release: 2013-01-14
Genre: Science
ISBN: 3527650342

Crystallization is a natural occurring process but also a process abundantly used in the industry. Crystallization can occur from a solution, from the melt or via deposition of material from the gas phase (desublimation). Crystals distinguish themself from liquids, gases and amorphous substances by the long-range order of its building blocks that entail the crystals to be formed of well-defined faces, and give rise to a large number of properties of the solid. Crystallization is used at some stage in nearly all process industries as a method of production, purification or recovery of solid materials. Crystallization is practiced on all scales: from the isolation of the first milligrams of a newly synthesized substance in the research laboratory to isolating products on the mulit-million tonne scale in industry. The book describes the breadth of crystallization operations, from isolation from a reaction broth to purification and finally to tailoring product properties. In the first section of the book, the basic mechanisms - nucleation, growth, attrition and agglomeration are introduced. It ensures an understanding of supersaturation, the driving force of crystallization. Furthermore, the solubility of the substance and its dependences on process conditions and the various techniques of crystallization and their possibilities and limitations are discussed. Last but not least, the first part includes an intensive treatment of polymorphism . The second part builds on the basics, exploring how crystallization processes can be developed, either batch-wise or continuous, from solution or from the melt. A discussion of the purification during crystallization serves as a link between the two sections, where practical aspects and an insight using theoretical concepts are combined. Mixing and its influence on the crystallization as well as the mutual interference of down-stream processes with the crystallization are also treated. Finally, techniques to characterize the crop are discussed. The third part of the book is dedicated to accounts of actual developments and of carried-out crystallizations. Typical pitfalls and strategies to avoid these as well as the design of robust processes are presented.

14th International Symposium on Industrial Crystallization

14th International Symposium on Industrial Crystallization
Author:
Publisher: IChemE
Total Pages: 2454
Release: 1999
Genre: Chemical engineering
ISBN: 0852954247

This conference provides a forum for discussion of the advances in the theory and practice of crystallization as it relates to the production of bulk crystalline materials.

Industrial Crystallization

Industrial Crystallization
Author: Alison Lewis
Publisher: Cambridge University Press
Total Pages: 354
Release: 2015-07-02
Genre: Technology & Engineering
ISBN: 1316299082

Bridging the gap between theory and practice, this text provides the reader with a comprehensive overview of industrial crystallization. Newcomers will learn all of the most important topics in industrial crystallization, from key concepts and basic theory to industrial practices. Topics covered include the characterization of a crystalline product and the basic process design for crystallization, as well as batch crystallization, measurement techniques, and details on precipitation, melt crystallization and polymorphism. Each chapter begins with an introduction explaining the importance of the topic, and is supported by homework problems and worked examples. Real world case studies are also provided, as well as new industry-relevant information, making this is an ideal resource for industry practitioners, students, and researchers in the fields of industrial crystallization, separation processes, particle synthesis, and particle technology.

Industrial Crystallization

Industrial Crystallization
Author: J. Mullin
Publisher: Springer Science & Business Media
Total Pages: 457
Release: 2012-12-06
Genre: Science
ISBN: 1461572584

Industrial Crystallization Symposia have been organized by the Crystallization Research Group at the Czechoslovak Research Institute for Inorganic Chemistry, Usti nad Labem, since 1960. Over the years, the increasing popularity of the unit operation of crystallization has been clearly demonstrated by the steady increase in numbers of both the papers presented and the attendances at the meetings. The 6th Symposium (1-3 September 1975) was organized jointly with the European Federation of Chemical Engineering Working Party on Crystallization, and the 44 papers presented were arranged into four sessions - A: Secondary Nucleation, B: Crystal Growth Kinetics, C: Crystal Habit Modification, D: Crystallizer Design, E: Indus trial Crystallizer Operation and Case Studies. The same groupings are preserved in this edited version of the proceedings. This is the first time that the Industrial Crystallization Symposium papers have appeared in one volume. After the 5th (1972) Symposium, authors we.re encouraged to submit their papers to an international journal specializing in crystallization. However, the results were not altogether satisfactory in that less than one third of the papers presented at the meeting were offered for consideration. This time, therefore, the organizing committee decided to attempt to keep the papers together by making arrangements for their pUblication by Plenum Press.

Melt Crystallization Technology

Melt Crystallization Technology
Author: Tine Arkenbout-de Vroome
Publisher: Routledge
Total Pages: 400
Release: 2021-01-31
Genre: Technology & Engineering
ISBN: 1351432230

From the Author's Preface: There is a growing demand for ultrapure organic compounds such as fine chemicals, pharmaceuticals, and basic materials for use in the polymer industry. . . . In quite a number of cases, it is difficult or impossible to manufacture ultrapure organics efficiently using conventional separation techniques such as distillation. Moreover, conventional techniques usually require large amounts of energy. To improve the purification efficiency of organics, special techniques based on crystallization from the melt have been developed. Melt crystallization meets industry's need for a highly selective separation process for organic compounds which operates at low enough temperatures to prevent thermal degradation. Melt crystallization processes have the added advantage that they are energy-efficient and ecologically sound. Melt crystallization techniques appear to be particularly promising for upgrading organic materials and are one of the few routes that appear to be feasible for purifying starter materials for high-tech polymers. The aim of this book is to provide basic information on melt crystallization technology. . . . This monograph consists of three parts: 1. basic principles, 2. process options, and 3. technical equipment and applicability. This new book is the first unified guide and reference to an important chemical process technology. It is comprehensive and organized for easy reference. More than 150 diagrammatic representations, flow charts and photographs illustrate equipment and processes. More than 40 tables provide useful reference data.

Crystallization

Crystallization
Author: Marcello Andreeta
Publisher: BoD – Books on Demand
Total Pages: 582
Release: 2012-09-19
Genre: Science
ISBN: 9535107577

Crystallization is one of the most ancient and interdisciplinary topics of research known to mankind. Crystals can be organic or inorganic and may be produced from melts, liquid solutions, vapors or even in solid state. Notwithstanding its inherently high complexity, the crystallization process is part of our everyday lives, from ice making in our homes to the most state-of-the-art chemical and electronic industry. In this book, our purpose was to present new insights to the reader, as well as crucial and very useful information for researchers working in this field, while simultaneously creating a comprehensive text about crystallization processes which may serve as a starting point for people with different backgrounds.