Electrochemical Methods for the Micro- and Nanoscale

Electrochemical Methods for the Micro- and Nanoscale
Author: Jochen Kieninger
Publisher: Walter de Gruyter GmbH & Co KG
Total Pages: 404
Release: 2022-02-21
Genre: Technology & Engineering
ISBN: 3110649756

Are electrochemical methods like asking the crystal ball? Once you read this book about electrochemistry on the micro- and nanoscale, you know it better. This textbook presents the essentials of electrochemical theory, sheds light on the instrumentation, including details on the electronics, and in the second part, discusses a wide variety of classical and advanced methods. The third part of the book covers how to apply the techniques for selected aspects of material science, microfabrication, nanotechnology, MEMS, NEMS, and energy applications. With this book, you will be able to successfully apply the methods in the fields of sensors, neurotechnology, biomedical engineering, and electrochemical energy systems. Undergraduate or Master students can read the book linearly as a comprehensive textbook. For Ph.D. students, postdoctoral researchers as well as for researchers in industry, the book will help by its clear structure to get fast answers from a specific section.

Nanoscale Electrochemistry

Nanoscale Electrochemistry
Author: Andrew J. Wain
Publisher: Elsevier
Total Pages: 580
Release: 2021-09-14
Genre: Technology & Engineering
ISBN: 0128200561

Nanoscale Electrochemistry focuses on challenges and advances in electrochemical nanoscience at solid–liquid interfaces, highlighting the most prominent developments of the last decade. Nanotechnology has had a tremendous effect on the multidisciplinary field of electrochemistry, yielding new fundamental insights that have broadened our understanding of interfacial processes and stimulating new and diverse applications. The book begins with a tutorial chapter to introduce the principles of nanoscale electrochemical systems and emphasize their unique behavior compared with their macro/microscopic counterparts. Building on this, the following three chapters present analytical applications, such as sensing and electrochemical imaging, that are familiar to the traditional electrochemist but whose extension to the nanoscale is nontrivial and reveals new chemical information. The subsequent three chapters present exciting new electrochemical methodologies that are specific to the nanoscale, including "single entity"-based methods and surface-enhanced electrochemical spectroscopy. These techniques, now sufficiently mature for exposition, have paved the way for major developments in our understanding of solid–liquid interfaces and continue to push electrochemical analysis toward atomic-length scales. The final three chapters address the rich overlap between electrochemistry and nanomaterials science, highlighting notable applications in energy conversion and storage. This is an important reference for both academic and industrial researchers who are seeking to learn more about how nanoscale electrochemistry has developed in recent years. - Outlines the major applications of nanoscale electrochemistry in energy storage, spectroscopy and biology - Summarizes the major principles of nanoscale electrochemical systems, exploring how they differ from similar system types - Discusses the major challenges of electrochemical analysis at the nanoscale

Electrochemical Methods

Electrochemical Methods
Author: Cynthia G. Zoski
Publisher: John Wiley & Sons
Total Pages: 214
Release: 2024-12-04
Genre: Science
ISBN: 1119524067

Provides students with solutions to problems in the 3rd edition of the classic textbook Electrochemical Methods: Fundamentals and Applications Electrochemical Methods is a popular textbook on electrochemistry that takes the reader from the most basic chemical and physical principles, through fundamentals of thermodynamics, kinetics, and mass transfer, all the way to a thorough treatment of all important experimental methods. Holistically, it offers comprehensive coverage of all important topics in the field. To aid in reader comprehension, exercises are included at the end of each chapter which extend concepts introduced in the text or show how experimental data are reduced to fundamental results. This book provides worked solutions for many of the end-of-chapter exercises and is a key resource for any student who makes use of the original textbook.

Corrosion Protection at the Nanoscale

Corrosion Protection at the Nanoscale
Author: Susai Rajendran
Publisher: Elsevier
Total Pages: 538
Release: 2020-03-12
Genre: Technology & Engineering
ISBN: 012819359X

Corrosion Protection at the Nanoscale explores fundamental concepts on how metals can be protected at the nanoscale by using both nanomaterials-based solutions, including nanoalloys, noninhibitors and nanocoatings. It is an important reference resource for both materials scientists and engineers wanting to find ways to create an efficient corrosion prevention strategy. Nanostructure materials have been widely used in many products, such as print electronics, contact, interconnection, implant, nanosensors and display units to lessen the impact of corrosion. Traditional methods for protection of metals include various techniques, such as coatings, inhibitors, electrochemical methods (anodic and cathodic protections), metallurgical design are covered in this book. Nanomaterials-based protective methods can offer many advantages over their traditional counterparts, such as protection for early-stage, higher corrosion resistance, better corrosion control. This book also outlines these advantages and discusses the challenges of implementing nanomaterials as corrosion protection agents on a wide scale.

Electrochemical Micromachining for Nanofabrication, MEMS and Nanotechnology

Electrochemical Micromachining for Nanofabrication, MEMS and Nanotechnology
Author: Bijoy Bhattacharyya
Publisher: William Andrew
Total Pages: 297
Release: 2015-04-10
Genre: Technology & Engineering
ISBN: 032335288X

Electrochemical Micromachining for Nanofabrication, MEMS and Nanotechnology is the first book solely dedicated to electrochemical micromachining (EMM). It begins with fundamentals, techniques, processes, and conditions, continuing with in-depth discussions of mechanisms of material removal, including an empirical model on the material removal rate for EMM (supported by experimental validation). The book moves next to construction-related features of EMM setup suitable for industrial micromachining applications, varying types of EMM, and the latest developments in the improvement of EMM setup. Further, it covers power supply, roll of electrolyte, and other major factors influencing EMM processes, and reports research findings concerning the improvement of machining accuracy and efficiency. Finally, the book devotes a chapter to the design and development of micro-tools, one of the most vital components in EMM. - Covers the generation of micro features used for advanced engineering of materials for fabrication of MEMS, microsystems and other micro-engineering applications - Explores the trend of decreasing size of fabricated devices, reflected in coverage of generation of high-precision nano-features on metal and semiconductors utilizing SPM, STM, and AFM, and nanotechnology aspects of EMM - Describes nanofabrication utilizing anodic dissolutions for mass manufacturing by overcoming obstacles utilizing electrochemical microsystem technology (EMST) and electrochemical nanotechnology (ENT)

Handbook of Electrochemistry

Handbook of Electrochemistry
Author: Cynthia G. Zoski
Publisher: Elsevier
Total Pages: 935
Release: 2007-02-07
Genre: Science
ISBN: 0444519580

Electrochemistry plays a key role in a broad range of research and applied areas including the exploration of new inorganic and organic compounds, biochemical and biological systems, corrosion, energy applications involving fuel cells and solar cells, and nanoscale investigations. The Handbook of Electrochemistry serves as a source of electrochemical information, providing details of experimental considerations, representative calculations, and illustrations of the possibilities available in electrochemical experimentation. The book is divided into five parts: Fundamentals, Laboratory Practical, Techniques, Applications, and Data. The first section covers the fundamentals of electrochemistry which are essential for everyone working in the field, presenting an overview of electrochemical conventions, terminology, fundamental equations, and electrochemical cells, experiments, literature, textbooks, and specialized books. Part 2 focuses on the different laboratory aspects of electrochemistry which is followed by a review of the various electrochemical techniques ranging from classical experiments to scanning electrochemical microscopy, electrogenerated chemiluminesence and spectroelectrochemistry. Applications of electrochemistry include electrode kinetic determinations, unique aspects of metal deposition, and electrochemistry in small places and at novel interfaces and these are detailed in Part 4. The remaining three chapters provide useful electrochemical data and information involving electrode potentials, diffusion coefficients, and methods used in measuring liquid junction potentials. * serves as a source of electrochemical information * includes useful electrochemical data and information involving electrode potentials, diffusion coefficients, and methods used in measuring liquid junction potentials * reviews electrochemical techniques (incl. scanning electrochemical microscopy, electrogenerated chemiluminesence and spectroelectrochemistry)

Applied Electrochemistry

Applied Electrochemistry
Author: Krystyna Jackowska
Publisher: Walter de Gruyter GmbH & Co KG
Total Pages: 404
Release: 2024-08-19
Genre: Science
ISBN: 311116098X

This book introduces the main aspects of modern applied electrochemistry. Starting with the basics of thermodynamic background, structure of interfaces and selected techniques used in analytical and material chemistry, the authors address the principles of electrochemistry in material science: corrosion, electrocatalysis, electrodeposition, energy storage and conversion. The application of nanostructured materials in these processes, as well as interfacing of electrochemistry with biology and medicine is discussed. The final part of the book is devoted to photoelectrochemistry and solar energy conversion in photoelectrochemical cells of various types. The goal of this book is to show that electrochemistry has many applications, not only for understanding of various phenomena in nowadays life but also in practical devices and can stimulate new science-enabled technologies, nourishing leaps from bench-top to large-scale industries, providing also means for protecting our environment. Creates a snapshot of the most important problems in applied electrochemistry and guides how to solve them. Gives an overview of the processes running during corrosion, electrodeposition and electrocatalysis. Focuses mainly on graduate students and those scientists who want to get a solid background knowledge of applied electrochemistry.

Electrochemical Sensors, Biosensors and their Biomedical Applications

Electrochemical Sensors, Biosensors and their Biomedical Applications
Author: Xueji Zhang
Publisher: Academic Press
Total Pages: 625
Release: 2011-04-28
Genre: Science
ISBN: 008055489X

This book broadly reviews the modem techniques and significant applications of chemical sensors and biosensors. Chapters are written by experts in the field – including Professor Joseph Wang, the most cited scientist in the world and renowned expert on sensor science who is also co-editor. Each chapter provides technical details beyond the level found in typical journal articles, and explores the application of chemical sensors and biosensors to a significant problem in biomedical science, also providing a prospectus for the future.This book compiles the expert knowledge of many specialists in the construction and use of chemical sensors and biosensors including nitric oxide sensors, glucose sensors, DNA sensors, hydrogen sulfide sensors, oxygen sensors, superoxide sensors, immuno sensors, lab on chip, implatable microsensors, et al. Emphasis is laid on practical problems, ranging from chemical application to biomedical monitoring and from in vitro to in vivo, from single cell to animal to human measurement. This provides the unique opportunity of exchanging and combining the expertise of otherwise apparently unrelated disciplines of chemistry, biological engineering, and electronic engineering, medical, physiological. - Provides user-oriented guidelines for the proper choice and application of new chemical sensors and biosensors - Details new methodological advancements related to and correlated with the measurement of interested species in biomedical samples - Contains many case studies to illustrate the range of application and importance of the chemical sensors and biosensors

Scanning Electrochemical Microscopy

Scanning Electrochemical Microscopy
Author: Allen J. Bard
Publisher: CRC Press
Total Pages: 619
Release: 2022-07-29
Genre: Science
ISBN: 1000584054

Because of its simplicity of use and quantitative results, Scanning Electrochemical Microscopy (SECM) has become an indispensable tool for the study of surface reactivity. The fast expansion of the SECM field over several years has been fueled by the introduction of new probes, commercially available instrumentation, and new practical applications. Scanning Electrochemical Microscopy, Third Edition offers essential background and in-depth overviews of specific applications in self-contained chapters. The vitality and growing popularity of SECM over the past 30+ years have largely been determined by its versatility and capability to remain useful in the changing scientific and technological environments. New applications reported during the last decade reflect significant current activity in biomedical and energy-related research. This thoroughly updated edition provides up-to-date comprehensive reviews of different aspects of SECM. New chapters by renowned professionals in the field cover recent advances in different areas of SECM including nanoSECM, surface reactions and films, batteries, and fuel cells. Expanded coverage of electrocatalysis and surface interrogation as well as photoelectrochemistry and photoelectrocatalysis are also provided. Useful for a broad range of interdisciplinary research—from biological systems to nanopatterning—this book is invaluable to all interested in learning and applying SECM.

Advances in Superhydrophobic Coatings

Advances in Superhydrophobic Coatings
Author: Viswanathan S Saji
Publisher: Royal Society of Chemistry
Total Pages: 512
Release: 2023-09-08
Genre: Technology & Engineering
ISBN: 1837670048

Superhydrophobic coatings have attracted substantial scientific research in recent years due to their real-world applications in a variety of fields including anti-corrosion, anti-icing, anti-fogging, oil separation and self-cleaning materials. Several approaches and methods have been used in developing superhydrophobic coatings on different substrates. This book guides readers through their fabrication and application, representing the latest significant advances in this important topic. Split into four sections, Part One concentrates on the fundamental principles of surface wettability and superhydrophobicity, before moving into Part Two and Part Three, which focus on different aspects of superhydrophobic coatings based on the materials used for fabrication and the substrate on which the coating is applied. Finally, Part Four focuses on the applications of these coatings. This book will serve as a valuable reference for graduate students, researchers and industrial practitioners in multiple industries working on surface wettability, materials chemistry and coatings related technologies.