Crystallization And Precipitation
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Author | : G L Strathdee |
Publisher | : Elsevier |
Total Pages | : 332 |
Release | : 2016-12-05 |
Genre | : Technology & Engineering |
ISBN | : 1483191109 |
Crystallization and Precipitation is a collection of papers that discusses the advancement in crystallization and precipitation technology. The titles assess the relative state of evolution of the science, engineering and practice in crystallization and precipitation. The coverage of the text includes chemical reactor approach to crystallizer analysis; uranium refining by uranyl nitrate hexahydrate crystallization; and valorization of liquid effluents by crystallization of sodium sulfate. The selection also covers precipitation of ferric arsenate from acid solutions; precipitation of silver on natural and synthetic sulphides theory and prospects of industrial use; and precipitation and its alternatives in the hydrometallurgy of gold. The book will be of great use to researchers and professionals who utilizes the mineral processes of crystallization and precipitation.
Author | : A. Mersmann |
Publisher | : CRC Press |
Total Pages | : 847 |
Release | : 2001-05-08 |
Genre | : Science |
ISBN | : 0824745116 |
This handbook seeks to facilitate the selection, design and operation of large-scale industrial crystallizers that process crystals with the proper size distribution, shape and purity sought. This second edition offers results on direct-contact cooling crystallization.
Author | : Alison Lewis |
Publisher | : Cambridge University Press |
Total Pages | : 354 |
Release | : 2015-07-02 |
Genre | : Technology & Engineering |
ISBN | : 1316299082 |
Bridging the gap between theory and practice, this text provides the reader with a comprehensive overview of industrial crystallization. Newcomers will learn all of the most important topics in industrial crystallization, from key concepts and basic theory to industrial practices. Topics covered include the characterization of a crystalline product and the basic process design for crystallization, as well as batch crystallization, measurement techniques, and details on precipitation, melt crystallization and polymorphism. Each chapter begins with an introduction explaining the importance of the topic, and is supported by homework problems and worked examples. Real world case studies are also provided, as well as new industry-relevant information, making this is an ideal resource for industry practitioners, students, and researchers in the fields of industrial crystallization, separation processes, particle synthesis, and particle technology.
Author | : Allan Myerson |
Publisher | : Butterworth-Heinemann |
Total Pages | : 329 |
Release | : 2002-01-08 |
Genre | : Technology & Engineering |
ISBN | : 0080533515 |
Crystallization is an important separation and purification process used in industries ranging from bulk commodity chemicals to specialty chemicals and pharmaceuticals. In recent years, a number of environmental applications have also come to rely on crystallization in waste treatment and recycling processes.The authors provide an introduction to the field of newcomers and a reference to those involved in the various aspects of industrial crystallization. It is a complete volume covering all aspects of industrial crystallization, including material related to both fundamentals and applications. This new edition presents detailed material on crystallization of biomolecules, precipitation, impurity-crystal interactions, solubility, and design.Provides an ideal introduction for industrial crystallization newcomers Serves as a worthwhile reference to anyone involved in the fieldCovers all aspects of industrial crystallization in a single, complete volume
Author | : Alan G. Jones |
Publisher | : Butterworth-Heinemann |
Total Pages | : 362 |
Release | : 2002-04-24 |
Genre | : Science |
ISBN | : 0750655208 |
Particulate Crystal Characteristics; Fluid-particle Transport Processes; Crystallization Principles and Techniques; Crystal Formation Processes; Crystallizer Design and Operation; Solid-Liquid Separation Processes; Design of Crystallization Process Systems.
Author | : Marcello Andreeta |
Publisher | : BoD – Books on Demand |
Total Pages | : 582 |
Release | : 2012-09-19 |
Genre | : Science |
ISBN | : 9535107577 |
Crystallization is one of the most ancient and interdisciplinary topics of research known to mankind. Crystals can be organic or inorganic and may be produced from melts, liquid solutions, vapors or even in solid state. Notwithstanding its inherently high complexity, the crystallization process is part of our everyday lives, from ice making in our homes to the most state-of-the-art chemical and electronic industry. In this book, our purpose was to present new insights to the reader, as well as crucial and very useful information for researchers working in this field, while simultaneously creating a comprehensive text about crystallization processes which may serve as a starting point for people with different backgrounds.
Author | : Terese M. Bergfors |
Publisher | : Internat'l University Line |
Total Pages | : 505 |
Release | : 2009 |
Genre | : Medical |
ISBN | : 0972077448 |
Author | : J. Mullin |
Publisher | : Springer Science & Business Media |
Total Pages | : 457 |
Release | : 2012-12-06 |
Genre | : Science |
ISBN | : 1461572584 |
Industrial Crystallization Symposia have been organized by the Crystallization Research Group at the Czechoslovak Research Institute for Inorganic Chemistry, Usti nad Labem, since 1960. Over the years, the increasing popularity of the unit operation of crystallization has been clearly demonstrated by the steady increase in numbers of both the papers presented and the attendances at the meetings. The 6th Symposium (1-3 September 1975) was organized jointly with the European Federation of Chemical Engineering Working Party on Crystallization, and the 44 papers presented were arranged into four sessions - A: Secondary Nucleation, B: Crystal Growth Kinetics, C: Crystal Habit Modification, D: Crystallizer Design, E: Indus trial Crystallizer Operation and Case Studies. The same groupings are preserved in this edited version of the proceedings. This is the first time that the Industrial Crystallization Symposium papers have appeared in one volume. After the 5th (1972) Symposium, authors we.re encouraged to submit their papers to an international journal specializing in crystallization. However, the results were not altogether satisfactory in that less than one third of the papers presented at the meeting were offered for consideration. This time, therefore, the organizing committee decided to attempt to keep the papers together by making arrangements for their pUblication by Plenum Press.
Author | : Angelo Chianese |
Publisher | : John Wiley & Sons |
Total Pages | : 253 |
Release | : 2012-04-06 |
Genre | : Science |
ISBN | : 3527645179 |
Crystallization is an important technique for separation and purification of substances as well as for product design in chemical, pharmaceutical and biotechnological process industries. This ready reference and handbook draws on research work and industrial practice of a large group of experts in the various areas of industrial crystallization processes, capturing the essence of current trends, the markets, design tools and technologies in this key field. Along the way, it outlines trouble free production, provides laboratory controls, analyses case studies and discusses new challenges. First the instrumentation and techniques used to measure the crystal size distribution, the nucleation and solubility points, and the chemical composition of the solid and liquid phase are outlined. Then the main techniques adopted to control industrial crystallizers, starting from fundamental approaches to the most advanced ones, including the multivariable predictive control are described. An overview of the main crystallizer types is given with details of the main control schemes adopted in industry as well as the more suitable sensors and actuators.
Author | : Wolfgang Beckmann |
Publisher | : John Wiley & Sons |
Total Pages | : 370 |
Release | : 2013-01-14 |
Genre | : Science |
ISBN | : 3527650342 |
Crystallization is a natural occurring process but also a process abundantly used in the industry. Crystallization can occur from a solution, from the melt or via deposition of material from the gas phase (desublimation). Crystals distinguish themself from liquids, gases and amorphous substances by the long-range order of its building blocks that entail the crystals to be formed of well-defined faces, and give rise to a large number of properties of the solid. Crystallization is used at some stage in nearly all process industries as a method of production, purification or recovery of solid materials. Crystallization is practiced on all scales: from the isolation of the first milligrams of a newly synthesized substance in the research laboratory to isolating products on the mulit-million tonne scale in industry. The book describes the breadth of crystallization operations, from isolation from a reaction broth to purification and finally to tailoring product properties. In the first section of the book, the basic mechanisms - nucleation, growth, attrition and agglomeration are introduced. It ensures an understanding of supersaturation, the driving force of crystallization. Furthermore, the solubility of the substance and its dependences on process conditions and the various techniques of crystallization and their possibilities and limitations are discussed. Last but not least, the first part includes an intensive treatment of polymorphism . The second part builds on the basics, exploring how crystallization processes can be developed, either batch-wise or continuous, from solution or from the melt. A discussion of the purification during crystallization serves as a link between the two sections, where practical aspects and an insight using theoretical concepts are combined. Mixing and its influence on the crystallization as well as the mutual interference of down-stream processes with the crystallization are also treated. Finally, techniques to characterize the crop are discussed. The third part of the book is dedicated to accounts of actual developments and of carried-out crystallizations. Typical pitfalls and strategies to avoid these as well as the design of robust processes are presented.