Capillary Gas Chromatography

Capillary Gas Chromatography
Author: David W. Grant
Publisher:
Total Pages: 308
Release: 1996-03-19
Genre: Science
ISBN:
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Analytical techniques based on separation processes, such as chromatography and electrophoresis, are finding a growing range of applications in chemical, pharmaceutical and clinical laboratories. This series provides the analyst in these laboratories with well focused books covering individual techniques, so that they can be applied more efficiently and effectively to contemporary analytical problems. Capillary gas chromatography is one of the most powerful separation tools available to analysts working in a wide diversity of disciplines. Capillary Gas Chromatography will give practising analysts a sound theoretical and practical knowledge of the subject, giving a thorough account of the many fascinating and important developments occurring in the field in recent years. The theory is presented with practical applications in mind. Common problems encountered when using this technique, and the means of overcoming them are also presented. Capillary Gas Chromatography will be of great practical use to analytical chemists using the technique, including those in the pharmaceutical, food and beverage, environmental, clinical, and petrochemical industries. It will also be invaluable for graduate students and researchers involved in the need to separate complex mixtures.

Gas Phase Chromatography

Gas Phase Chromatography
Author: Rudolf Kaiser
Publisher: Springer Science & Business Media
Total Pages: 129
Release: 2012-12-06
Genre: Science
ISBN: 1468482947
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THE remarkable capabilities of capillary gas partition chromatography (or, in short, capillary chromatography) are beyond all doubt. In spite of this, difficulties are continually arising in the experimental realization of this interesting development of gas chromatography, and this hinders the rapid acceptance of these methods. For this reason, in the present work I have dealt with experimental and practical problems rather than with theoretical aspects, hoping that this may serve to remove many of the problems con cerned. The present publication is based on experimental work carried out in productive collaboration with my teachers and colleagues, to whom I owe a great deal. I should like to thank the following for their valuable assistance and stimulating suggestions: Professor E. Cremer, Dr. H. Kienitz and his colleagues, Professor A. I. M. Keulemans, Dr. I. Halasz, and in particular Mr. D. H. Desty and Dr. R. P. W. Scott. I should also like to thank the management of the Badische Anilin- und Sodafabrik AG, Ludwigshafen, for their generous support and for per mission to publish this book. The outstanding co-operation of the Verlag Bibliographisches Institut, Mannheim, was for me a particular pleasure.

A Practical Guide to the Care, Maintenance and Troubleshooting of Capillary Gas Chromatographic Systems

A Practical Guide to the Care, Maintenance and Troubleshooting of Capillary Gas Chromatographic Systems
Author: Dean Rood
Publisher: Wiley-VCH
Total Pages: 352
Release: 1999-03-02
Genre: Science
ISBN:
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Dean Rood A Practical Guide to the Care, Maintenance, and Troubleshooting of Capillary Gas Chromatographic Systems Third, Revised Edition The field of gas chromatography continues the evolutionary process. This is well demonstrated by the continuous series of developments — in columns, equipment, apparatus, techniques, and applications — that have occured since the publication of the first edition of this very successful offering. Problems experienced by users differ from case to case, and these differences sometimes necessitate different approaches to care, maintenance, and trouble-shooting. This book is intended for the average GC user and not for those whose entire life revolves around capillary gas chromatography. The topics covered within these pages are based on the most common problems, questions, and misconceptions about capillary gas chromatography. These topics have been assembled and presented in a unique, practical, and concise format suitable even for the most inexperienced user. The author has not changed his successful approach to the topic in the present third edition. Instead, he has focused on updating and correcting the text of the widely acclaimed second edition.

Gas Chromatography with Glass Capillary Columns

Gas Chromatography with Glass Capillary Columns
Author: Walter Jennings
Publisher: Elsevier
Total Pages: 193
Release: 2012-12-02
Genre: Science
ISBN: 0323141064
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Gas Chromatography with Glass Capillary Columns describes glass capillary technology and the selection, installation, evaluation, and use of glass open tubular columns for gas chromatography. Discussions are organized around the glass capillary column; column coating and installation; inlet systems; measurement of column efficiency; temperature programming and carrier flow; and retention behavior. Column selection and stability and sample preparation are also covered. This text is comprised of 13 chapters; the first of which introduces the reader to the practical considerations involved in the selection, installation, evaluation, and use of high-resolution open tubular glass capillary columns, along with the theory of the chromatographic process. The discussion then turns to the influence of operating parameters and storage conditions on the interrelated forces involved in coating glass capillary columns; the dynamic and static techniques of column coating; and design defects in the inlet system caused by excessive volume and dead space. The chapters that follow focus on general considerations in column attachment, measurement of column efficiency, and retention behavior of carrier gas, along with the operating temperature of the column, the choice of carrier gas, and carrier gas velocity. This book also looks at the factors that affect column stability, materials of restricted volatility, and some applications of glass capillary gas chromatography. This reference material is intended primarily for students and researchers interested in gas chromatography with glass capillary columns.

Columns for Gas Chromatography

Columns for Gas Chromatography
Author: Eugene F. Barry
Publisher: John Wiley & Sons
Total Pages: 315
Release: 2007-04-27
Genre: Science
ISBN: 0470114177
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Choosing the right column is key in Gas Chromatography Gas Chromatography (GC) is the most widely used method for separating and analyzing a wide variety of organic compounds and gases. There have been many recent advancements in both packed column and capillary column GC. With numerous options and considerations, selecting the right column can be complicated. This resource provides essential guidance for scientists and technicians, including: Methods of choosing both capillary and packed columns Selection of dimensions (column length, I.D., film thickness, etc.) and type of column Guidelines for proper connections of the column to the injector and detector United States Pharmacopeia and National Formulary chromatographic methods ASTM, EPA, NIOSH, and OSHA column selection specifications Information on the advantages of computer assistance in GC and multidimensional GC Comprehensive information on column oven temperature control Columns for Gas Chromatography: Performance and Selection is a hands-on reference for scientists and technicians using GC.