Over the most recent couple of years, the importance of undergraduate technical education has grown amid a huge industrial revolution in our country. More refined and recently discovered super-specific topics are being introduced instead of old ones while modifying the course curriculum. In the new course curriculum, more noteworthy accentuation is laid on the basic science subjects and, on the need, to develop in-depth knowledge about the fundamentals of any particular area of academic interest. Keeping all this in mind, and utilizing my long experience as a teacher in a technical college under a technical university, I have ventured to write this book titled, Engineering Chemistry Laboratory Manual. In this book, all experiments are explained as per the JNTU syllabus for the first-year students of B.Tech. These are supplemented with theoretical explanations followed by procedure description, tabulation, calculation, sample calculation, and finally a series of possible viva-voce questions and their answers relating to that experiment. This book will certainly help all B.Tech./B.E. students to do well in their viva voce while completing their experiments cum examinations. It will also serve as a textbook in Chemistry practical examinations for any student in the laboratory. I sincerely hope that this book will receive full appreciation from both students and teachers.