X-ray Scattering of Synthetic Polymers

X-ray Scattering of Synthetic Polymers
Author: F. J. Baltá-Calleja
Publisher: Elsevier Publishing Company
Total Pages: 344
Release: 1989
Genre: Science
ISBN:

X-Ray scattering is one of the most powerful tools in the study of the structure of the wide class of polymeric materials in which partial crystallization occurs. The scattering at wide angles provides information on the unit cell variations, the crystallinity, the crystalline perfection and the orientation of the crystallites, whereas the scattering at small angles is specially suited to a description of the crystalline-amorphous morphology. As a result of scientific advances and industrial interest in polymers, progress in constantly being made in the application of X-ray scattering to these materials. This book describes the current state-of-the-art of the application of X-ray scattering to the study of solid polymer materials. As well as chapters on theory and instrumentation, the book covers subjects concerning the measurement of lattice constants, the crystalline perfection, the degree of crystallinity and the description of preferred orientation. In addition, special emphasis is given to the study of the crystalline morphology with the aid of small-angle X-ray scattering, giving both theoretical background and practical information.

Polymer Characterization

Polymer Characterization
Author: Dan Campbell
Publisher: CRC Press
Total Pages: 492
Release: 2017-12-21
Genre: Technology & Engineering
ISBN: 1482268361

Discerning the properties of polymers and polymer-based materials requires a good understanding of characterization. This revised and updated text provides a comprehensive survey of characterization methods within its simple, concise chapters. Polymer Characterization: Physical Techniques, provides an overview of a wide variety of characterization methods, which makes it an excellent textbook and reference. It starts with a description of basic polymer science, providing a solid foundation from which to understand the key physical characterization techniques. The authors explain physical principles without heavy theory and give special emphasis to the application of the techniques to polymers, with plenty of illustrations. Topics covered include molecular weight determination, molecular and structural characterization by spectroscopic techniques, morphology and structural characterization by microscopy and diffraction, and thermal analysis. This edition contains a new chapter on surface analysis as well as some revised problems and solutions. The concise treatment of each topic offers even those with little prior knowledge of the subject an accessible source to relevant, simple descriptions in a well-organized format.

Characterization of Polymer Blends

Characterization of Polymer Blends
Author: Sabu Thomas
Publisher: John Wiley & Sons
Total Pages: 972
Release: 2015-02-09
Genre: Science
ISBN: 3527331530

Filling the gap for a reference dedicated to the characterization of polymer blends and their micro and nano morphologies, this book provides comprehensive, systematic coverage in a one-stop, two-volume resource for all those working in the field. Leading researchers from industry and academia, as well as from government and private research institutions around the world summarize recent technical advances in chapters devoted to their individual contributions. In so doing, they examine a wide range of modern characterization techniques, from microscopy and spectroscopy to diffraction, thermal analysis, rheology, mechanical measurements and chromatography. These methods are compared with each other to assist in determining the best solution for both fundamental and applied problems, paying attention to the characterization of nanoscale miscibility and interfaces, both in blends involving copolymers and in immiscible blends. The thermodynamics, miscibility, phase separation, morphology and interfaces in polymer blends are also discussed in light of new insights involving the nanoscopic scale. Finally, the authors detail the processing-morphology-property relationships of polymer blends, as well as the influence of processing on the generation of micro and nano morphologies, and the dependence of these morphologies on the properties of blends. Hot topics such as compatibilization through nanoparticles, miscibility of new biopolymers and nanoscale investigations of interfaces in blends are also addressed. With its application-oriented approach, handpicked selection of topics and expert contributors, this is an outstanding survey for anyone involved in the field of polymer blends for advanced technologies.

Basic X-ray Scattering for Soft Matter

Basic X-ray Scattering for Soft Matter
Author: Wilhelmus Hendrikus Jeu
Publisher: Oxford University Press
Total Pages: 149
Release: 2016
Genre: Science
ISBN: 0198728662

X-ray scattering is a well-established technique in materials science. The aim of this text is to explain basic principles and applications of x-ray scattering in a simple way using many practical examples followed by more elaborate case studies. It contains a separate chapter on the different types of order/disorder in soft matter that play such an important role in modern self-assembling systems. Finally the last chapter treats soft matter surfaces and thin film that are increasingly used in coatings and in many technological applications, such as liquid crystal displays and nanostructured block copolymer films

Polymer Synthesis and Characterization

Polymer Synthesis and Characterization
Author: Stanley R. Sandler
Publisher: Elsevier
Total Pages: 231
Release: 1998-05-21
Genre: Technology & Engineering
ISBN: 0080539211

This laboratory manual covers important techniques for polymer synthesis and characterization, and provides newcomers with a comprehensive introduction to the basic principles of highlighted techniques. The reader will benefit from the clear writing style and straightforward approach to fairly complex ideas. The book also provides references that the more advanced reader can use to obtain in-depth explanations of techniques. Polymer Synthesis and Characterization will serve as a useful resource for industrial technicians and researchers in polymer chemistry and physics, material science, and analytical chemistry. - Combines the extensive industrial and teaching experience of the authors - Introduces the user to the concept of "Good Manufacturing Practice" - Presents experiments that are representative of a wide variety of polymerization and characterization methods - Includes numerous references for more advanced students, technicians, and researcher

Molecular Characterization of Polymers

Molecular Characterization of Polymers
Author: Muhammad Imran Malik
Publisher: Elsevier
Total Pages: 670
Release: 2021-03-09
Genre: Technology & Engineering
ISBN: 012822598X

Molecular Characterization of Polymers presents a range of advanced and cutting-edge methods for the characterization of polymers at the molecular level, guiding the reader through theory, fundamentals, instrumentation, and applications, and supporting the end goal of efficient material selection and improved material performance. Each chapter focuses on a specific technique or family of techniques, including the different areas of chromatography, field flow fractionation, long chain branching, static and dynamic light scattering, mass spectrometry, NMR, X-Ray and neutron scattering, polymer dilute solution viscometry, microscopy, and vibrational spectroscopy. In each case, in-depth coverage explains how to successfully implement and utilize the technique. This practical resource is highly valuable to researchers and advanced students in polymer science, materials science, and engineering, and to those from other disciplines and industries who are unfamiliar with polymer characterization techniques. - Introduces a range of advanced characterization methods, covering aspects such as molecular weight, polydispersity, branching, composition, and tacticity - Enables the reader to understand and to compare the available technique, and implement the selected technique(s), with a view to improving properties of the polymeric material - Establishes a strong link between basic principles, characterization techniques, and real-life applications

Scattering Methods and their Application in Colloid and Interface Science

Scattering Methods and their Application in Colloid and Interface Science
Author: Otto Glatter
Publisher: Elsevier
Total Pages: 406
Release: 2018-01-08
Genre: Technology & Engineering
ISBN: 0128135816

Scattering Methods and their Application in Colloid and Interface Science offers an overview of small-angle X-ray and neutron scattering techniques (SAXS & SANS), as well as static and dynamic light scattering (SLS & DLS). These scattering techniques are central to the study of soft matter, such as colloidal dispersions and surfactant self-assembly. The theoretical concepts are followed by an overview of instrumentation and a detailed description of the evaluation techniques in the first part of the book. In the second part, several typical application examples are used to show the strength and limitations of these techniques. - Features the latest input from the world-leading expert with personal experience in all the fields covered (SAXS, SANS, SLS and DLS) - Includes unified notation throughout the book to enhance its readability - Provides—in a single source—scattering theory, evaluation of techniques and a variety of applications