Temperature Programmed Gas Chromatography
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| Author | : Harold M. McNair |
| Publisher | : John Wiley & Sons |
| Total Pages | : 195 |
| Release | : 2011-09-20 |
| Genre | : Science |
| ISBN | : 1118211200 |
The New Edition of the Well-Regarded Handbook on Gas Chromatography Since the publication of the highly successful first edition of Basic Gas Chromatography, the practice of chromatography has undergone several notable developments. Basic Gas Chromatography, Second Edition covers the latest in the field, giving readers the most up-to-date guide available, while maintaining the first edition's practical, applied approach to the subject and its accessibility to a wide range of readers. The text provides comprehensive coverage of basic topics in the field, such as stationary phases, packed columns and inlets, capillary columns and inlets, detectors, and qualitative and quantitative analysis. At the same time, the coverage also features key additions and updated topics including: Gas chromatography-mass spectrometry (GC-MS) Sampling methods Multidimensional gas chromatography Fast gas chromatography Gas chromatography analysis of nonvolatile compounds Inverse gas chromatography and pyrolysis gas chromatography Along with these new and updated topics, the references, resources, and Web sites in Basic Gas Chromatography have been revised to reflect the state of the field. Concise and fundamental in its coverage, Basic Gas Chromatography, Second Edition remains the standard handbook for everyone from undergraduates studying analytical chemistry to working industrial chemists.
| Author | : Leonid M. Blumberg |
| Publisher | : John Wiley & Sons |
| Total Pages | : 363 |
| Release | : 2011-09-22 |
| Genre | : Science |
| ISBN | : 3527632263 |
This book provides a comprehensive up-to-date overview of temperature-programmed gas chromatography (GC). The first part of the book introduces the reader to the basics concepts of GC, as well as the key properties of GC columns. The second part describes the mathematical and physical background of GC. In the third part, different aspects in the formation of a chromatogram are discussed, including retention times, peak spacing and peak widths. An invaluable reference for any chromatographer and analytical chemist, it provides all the answers to questions like: At what temperature does a solute elute in a temperature-programmed analysis? What is the value of the retention factor of eluting solute? How wide are the peaks? How large is the time distance between two peaks? How do all these parameters depend on the heating rate?
| Author | : Konrad Grob |
| Publisher | : John Wiley & Sons |
| Total Pages | : 480 |
| Release | : 2008-11-21 |
| Genre | : Science |
| ISBN | : 3527612882 |
This comprehensive and unique handbook of split and splitless injection techniques has been completely revised and updated. This new edition offers: - New insights concerning sample evaporation in the injector - Information about matrix effects - A new chapter on injector design The real processes within the injector are for the first time visualized and explained by the CD-ROM included in the book. Furthermore the reader will understand the concepts of injection techniques and get a knowledge of the sources of error. The handbook also includes many practical guidelines. From reviews of former editions: "This substantial book is on injection techniques alone, which ... demonstrates this can have many pitfalls ... no one should be allowed to direct a laboratory doing quantitative analysis by GC without first being thoroughly familar with this book ..." The Analyst "This is a detailed reference volume filled with practical suggestions and techniques for managing split and splitless injection in the day-to-day world of the working gas chromatographer. It will be useful ... for anyone who must work hands-on with GC." Journal of High Resolution Chromatography
| Author | : Katja Dettmer-Wilde |
| Publisher | : Springer |
| Total Pages | : 904 |
| Release | : 2014-11-05 |
| Genre | : Science |
| ISBN | : 3642546404 |
Gas chromatography continues to be one of the most widely used analytical techniques, since its applications today expand into fields such as biomarker research or metabolomics. This new practical textbook enables the reader to make full use of gas chromatography. Essential fundamentals and their implications for the practical work at the instrument are provided, as well as details on the instrumentation such as inlet systems, columns and detectors. Specialized techniques from all aspects of GC are introduced ranging from sample preparation, solvent-free injection techniques, and pyrolysis GC, to separation including fast GC and comprehensive GCxGC and finally detection, such as GC-MS and element-specific detection. Various fields of application such as enantiomer, food, flavor and fragrance analysis, physicochemical measurements, forensic toxicology, and clinical analysis are discussed as well as cutting-edge application in metabolomics is covered.
| Author | : Matthew S. Klee |
| Publisher | : Hewlett-Packard, Avondale Division |
| Total Pages | : 132 |
| Release | : 1990-02-01 |
| Genre | : Gas chromatography |
| ISBN | : 9781880313008 |
| Author | : Eric Stauffer |
| Publisher | : Academic Press |
| Total Pages | : 683 |
| Release | : 2007-12-10 |
| Genre | : Law |
| ISBN | : 0080556264 |
The study of fire debris analysis is vital to the function of all fire investigations, and, as such, Fire Debris Analysis is an essential resource for fire investigators. The present methods of analysis include the use of gas chromatography and gas chromatography-mass spectrometry, techniques which are well established and used by crime laboratories throughout the world. However, despite their universality, this is the first comprehensive resource that addresses their application to fire debris analysis.Fire Debris Analysis covers topics such as the physics and chemistry of fire and liquid fuels, the interpretation of data obtained from fire debris, and the future of the subject. Its cutting-edge material and experienced author team distinguishes this book as a quality reference that should be on the shelves of all crime laboratories. - Serves as a comprehensive guide to the science of fire debris analysis - Presents both basic and advanced concepts in an easily readable, logical sequence - Includes a full-color insert with figures that illustrate key concepts discussed in the text
| Author | : Leslie S. Ettre |
| Publisher | : Springer Science & Business Media |
| Total Pages | : 176 |
| Release | : 2012-12-06 |
| Genre | : Science |
| ISBN | : 1468406884 |
For my past sins, Leslie Ettre has given me the privilege of writing a few words to preface his excellent little book. It gives me great pleasure to do so, because of the many years of fruitful collabo ration we have had at Perkin-Elmer, because it is refreshing to see a treatise in gas chromatography in which the theoretical treatment has been bared to its essentials, without a mushrooming of formulae which, by means of an ever increasing number of parameters, account for more and more, and explain less and less, and because the author has recognized that the gas chromatographic column is a nearly passive element in its own right which deserves to have a treatise written nearly exclusively about it, just as electrical circuit theory can be discussed without elaborate references to vacuum tubes and meters. I wish this conscientiously written volume the success it deserves. M. J. E. GOLAY VII Preface Gas chromatography is a separation technique used primarily in analytical chemistry. Therefore, it is evident that special emphasis should be placed on that particular part of the apparatus in which the separation takes place. This part is the column, the heart of the gas chromatograph. The goal of researchers in the field of gas chromatography has been-from the beginning-to understand the separation process so that they might design columns with the best possible performance. Such investigation led M. J. E.
| Author | : Walter Jennings |
| Publisher | : Elsevier |
| Total Pages | : 270 |
| Release | : 2012-12-02 |
| Genre | : Science |
| ISBN | : 0323141072 |
Analytical Gas Chromatography is a free-standing introduction to and guide through the rapidly progressing field of analytical gas chromatography. The book is divided into 10 chapters that cover various aspects of analytical gas chromatography, from most advantageous column type to troubleshooting. The opening chapters of the book discuss the advantages of the open tubular column over the packed column. This topic is followed by significant chapters on various variables in the gas chromatographic process, including sample injection, stationary phase, carrier gas, and installation. The effect of changes in these variables on the solution elution order is also considered. A chapter also examines the influence of instrumental design features, such as excessive or unswept volumes in the flow path; suitability of the detection mode; and speed and fidelity of the data-handling equipment. The book also presents selected methods that have been employed to achieve better results for a given gas chromatographic problem. The application areas of gas chromatographic process, including food, flavor, fragrance, petroleum- and chemical-related, environment, biology, and medicine, are also presented. The concluding chapter addresses the basic troubleshooting knowledge and considers other chromatographic problems and methods for their rectification.
| Author | : Robert L. Grob, PhD |
| Publisher | : John Wiley & Sons |
| Total Pages | : 1059 |
| Release | : 2004-08-04 |
| Genre | : Science |
| ISBN | : 047165115X |
The bible of gas chromatography-offering everything the professional and the novice need to know about running, maintaining, and interpreting the results from GC Analytical chemists, technicians, and scientists in allied disciplines have come to regard Modern Practice of Gas Chomatography as the standard reference in gas chromatography. In addition to serving as an invaluable reference for the experienced practitioner, this bestselling work provides the beginner with a solid understanding of gas chromatographic theory and basic techniques. This new Fourth Edition incorporates the most recent developments in the field, including entirely new chapters on gas chromatography/mass spectrometry (GC/MS); optimization of separations and computer assistance; high speed or fast gas chromatography; mobile phase requirements: gas system requirements and sample preparation techniques; qualitative and quantitative analysis by GC; updated information on detectors; validation and QA/QC of chromatographic methods; and useful hints for good gas chromatography. As in previous editions, contributing authors have been chosen for their expertise and active participation in their respective areas. Modern Practice of Gas Chromatography, Fourth Edition presents a well-rounded and comprehensive overview of the current state of this important technology, providing a practical reference that will greatly appeal to both experienced chomatographers and novices.
| Author | : Peter Q Tranchida |
| Publisher | : Royal Society of Chemistry |
| Total Pages | : 492 |
| Release | : 2019-10-30 |
| Genre | : Science |
| ISBN | : 1788011279 |
Gas chromatography is widely used in applications involving food analysis. Typical applications pertain to the quantitative and/or qualitative analysis of food composition, natural products, food additives, and flavour and aroma components. Providing an up-to-date look at the significant advances in the technology, this book includes details on novel sample preparation processes; conventional, high-speed multidimensional gas chromatography systems, including preparative instrumentation; gas chromatography–olfactometry principles; and, finally, chemometrics principles and applications in food analysis. Aimed at providing the food researcher or analyst with detailed analytical information related to advanced gas chromatography technologies, this book is suitable for professionals and postgraduate students learning about the technique in the food industry and research.
