Basic Techniques of Preparative Organic Chemistry

Basic Techniques of Preparative Organic Chemistry
Author: William Sabel
Publisher: Elsevier
Total Pages: 207
Release: 2013-09-03
Genre: Science
ISBN: 1483213773

Basic Techniques of Preparative Organic Chemistry covers a detailed guide for carrying out the procedures commonly needed in preparative organic chemistry. The book discusses the nature of organic reactions; the basic principles of preparative organic chemistry; unit operations; and good laboratory practice. The text then provides a review of apparatus and equipment and describes the potential hazards involved in a chemical operation, such as toxicity, bodily injuries, smoking, fire, explosion, and implosion. Techniques and unit operations for carrying out a reaction and for isolating and purifying a reaction product; and the criteria for and methods of assessing purity are also considered. The book further tackles packing and storing products and samples and making reports and communications. Students taking organic chemistry courses will find the text useful.

Techniques in Organic Chemistry

Techniques in Organic Chemistry
Author: Jerry R. Mohrig
Publisher: Macmillan
Total Pages: 487
Release: 2010-01-06
Genre: Science
ISBN: 1429219564

"Compatible with standard taper miniscale, 14/10 standard taper microscale, Williamson microscale. Supports guided inquiry"--Cover.

High-resolution NMR Techniques in Organic Chemistry

High-resolution NMR Techniques in Organic Chemistry
Author: T. Claridge
Publisher: Elsevier
Total Pages: 408
Release: 1999-12-24
Genre: Science
ISBN: 9780080427997

From the initial observation of proton magnetic resonance in water and in paraffin, the discipline of nuclear magnetic resonance has seen unparalleled growth as an analytical method. Modern NMR spectroscopy is a highly developed, yet still evolving, subject which finds application in chemistry, biology, medicine, materials science and geology. In this book, emphasis is on the more recently developed methods of solution-state NMR applicable to chemical research, which are chosen for their wide applicability and robustness. These have, in many cases, already become established techniques in NMR laboratories, in both academic and industrial establishments. A considerable amount of information and guidance is given on the implementation and execution of the techniques described in this book.

Practical Synthetic Organic Chemistry

Practical Synthetic Organic Chemistry
Author: Stéphane Caron
Publisher: John Wiley & Sons
Total Pages: 870
Release: 2011-07-26
Genre: Science
ISBN: 1118093569

A hands-on guide to assist in the planning and execution of synthetic reactions in the laboratory Despite the maturity of organic chemistry, it can still be very challenging to identify optimal methods for synthetic transformations that perform as well in real-world manufacturing processes as they do in the laboratory. This detailed and accessible guide attempts to address this vexing issue and deliver proven methodologies practicing synthetic chemists will find valuable for identifying reaction conditions that work reliably over the broadest possible range of substrates. Practical Synthetic Organic Chemistry: Provides a practical guide to strategically planning and executing chemical syntheses for the bench chemist in industry Discusses information that is not common knowledge beyond the boundaries of process chemistry groups, such as the synthetic routes of selected contemporary pharmaceutical drugs and practical solvents, as well as green chemistry concepts Highlights key reactions, including substitutions, additions, eliminations, rearrangements, oxidations, and reductions Addresses basic principles, mechanisms, advantages and disadvantages of the methodology, and techniques for achieving laboratory success Incorporating such an extraordinary wealth of information on organic chemistry and its related fields into one complete volume distinguishes Practical Synthetic Organic Chemistry as an incomparable desktop reference for professionals and an invaluable study aid for students.

Techniques in Organic Chemistry

Techniques in Organic Chemistry
Author: Jerry R. Mohrig
Publisher: Macmillan
Total Pages: 436
Release: 2006
Genre: Science
ISBN: 9780716769354

Is the most comprehensive and detailed presentation of lab techniques available for organic chemistry students - and the least expensive. It combines specific instructions for 3 different kinds kinds of laboratory glassware and offers extensive coverage of spectroscopic techniques and a strong emphasis on safety issues.

Purification of Laboratory Chemicals

Purification of Laboratory Chemicals
Author: W.L.F. Armarego
Publisher: Elsevier
Total Pages: 627
Release: 2003-03-07
Genre: Technology & Engineering
ISBN: 0080515460

Now in its fifth edition, the book has been updated to include more detailed descriptions of new or more commonly used techniques since the last edition as well as remove those that are no longer used, procedures which have been developed recently, ionization constants (pKa values) and also more detail about the trivial names of compounds.In addition to having two general chapters on purification procedures, this book provides details of the physical properties and purification procedures, taken from literature, of a very extensive number of organic, inorganic and biochemical compounds which are commercially available. This is the only complete source that covers the purification of laboratory chemicals that are commercially available in this manner and format.* Complete update of this valuable, well-known reference* Provides purification procedures of commercially available chemicals and biochemicals* Includes an extremely useful compilation of ionisation constants

Practical Synthetic Organic Chemistry

Practical Synthetic Organic Chemistry
Author: Stéphane Caron
Publisher: John Wiley & Sons
Total Pages: 850
Release: 2020-02-05
Genre: Science
ISBN: 1119448859

This book is a hands-on guide for the organic chemist. Focusing on the most reliable and useful reactions, the chapter authors provide the information necessary for a chemist to strategically plan a synthesis, as well as repeat the procedures in the laboratory. Consolidates all the key advances/concepts in one book, covering the most important reactions in organic chemistry, including substitutions, additions, eliminations, rearrangements, oxidations, reductions Highlights the most important reactions, addressing basic principles, advantages/disadvantages of the methodology, mechanism, and techniques for achieving laboratory success Features new content on recent advances in CH activation, photoredox and electrochemistry, continuous chemistry, and application of biocatalysis in synthesis Revamps chapters to include new and additional examples of chemistry that have been demonstrated at a practical scale

Determination of Organic Structures by Physical Methods

Determination of Organic Structures by Physical Methods
Author: E. A. Braude
Publisher: Elsevier
Total Pages: 825
Release: 2013-10-22
Genre: Science
ISBN: 1483275728

Determination of Organic Structures by Physical Methods, Volume 1 focuses on the processes, methodologies, principles, and approaches involved in the determination of organic structures by physical methods, including infrared light absorption, thermodynamic properties, Raman spectra, and kinetics. The selection first elaborates on the phase properties of small molecules, equilibrium and dynamic properties of large molecules, and optical rotation. Discussions focus on simple acyclic compounds, carbohydrates, steroids, diffusion, viscosity, osmotic pressure, sedimentation velocity, melting and boiling points, and molar volume. The book then examines ultraviolet and visible light absorption, infrared light absorption, Raman spectra, and the theory of magnetic susceptibility. Concerns cover applications to the study of organic compounds, applications to the determination of structure, determination of thermodynamic properties, and experimental methods and evaluation of data. The text ponders on wave-mechanical theory, reaction kinetics, and dissociation constants, including dissociation of molecular addition compounds, principles of reaction kinetics, and valence-bond treatment of aromatic systems. The selection is a valuable source of data for researchers interested in the determination of organic structures by physical methods.