Structure Envelopes And Their Application In Structure Determination From Powder Diffraction Data
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| Author | : W. I. F. David |
| Publisher | : OUP Oxford |
| Total Pages | : 358 |
| Release | : 2006-08-03 |
| Genre | : Science |
| ISBN | : 0191525561 |
The art of solving a structure from powder diffraction data has developed rapidly over the last ten years to the point where numerous crystal structures, both organic and inorganic, have been solved directly from powder data. However, it is still an art and, in contrast to its single crystal equivalent, is far from routine. The art lies not only in the correct application of a specific experimental technique or computer program, but also in the selection of the optimal path for the problem at hand. Written and edited by experts active in the field, and covering both the fundamental and applied aspects of structure solution from powder diffraction data, this book guides both novices and experienced practitioners alike through the maze of possibilities.
| Author | : William I. F. David |
| Publisher | : OUP Oxford |
| Total Pages | : 358 |
| Release | : 2002 |
| Genre | : Language Arts & Disciplines |
| ISBN | : 0198500912 |
Our understanding of the properties of materials, from drugs and proteins to catalysts and ceramics, is almost always based on structural information. This book describes the new developments in the realm of powder diffraction which make it possible for scientists to obtain such information even from polycrystalline materials. Written and edited by experts active in the field, and covering both the fundamental and applied aspects of structure solution from powder diffraction data, this book guides both novices and experienced practitioners alike through the maze of possibilities.
| Author | : Ute Kolb |
| Publisher | : Springer |
| Total Pages | : 427 |
| Release | : 2012-12-20 |
| Genre | : Science |
| ISBN | : 9400755805 |
The polycrystalline and nanocrystalline states play an increasingly important role in exploiting the properties of materials, encompassing applications as diverse as pharmaceuticals, catalysts, solar cells and energy storage. A knowledge of the three-dimensional atomic and molecular structure of materials is essential for understanding and controlling their properties, yet traditional single-crystal X-ray diffraction methods lose their power when only polycrystalline and nanocrystalline samples are available. It is here that powder diffraction and single-crystal electron diffraction techniques take over, substantially extending the range of applicability of the crystallographic principles of structure determination. This volume, a collection of teaching contributions presented at the Crystallographic Course in Erice in 2011, clearly describes the fundamentals and the state-of-the-art of powder diffraction and electron diffraction methods in materials characterisation, encompassing a diverse range of disciplines and materials stretching from archeometry to zeolites. As such, it is a comprehensive and valuable resource for those wishing to gain an understanding of the broad applicability of these two rapidly developing fields.
| Author | : R E Dinnebier |
| Publisher | : Royal Society of Chemistry |
| Total Pages | : 525 |
| Release | : 2015-11-09 |
| Genre | : Science |
| ISBN | : 1782625992 |
Powder diffraction is a widely used scientific technique in the characterization of materials with broad application in materials science, chemistry, physics, geology, pharmacology and archaeology. Powder Diffraction: Theory and Practice provides an advanced introductory text about modern methods and applications of powder diffraction in research and industry. The authors begin with a brief overview of the basic theory of diffraction from crystals and powders. Data collection strategies are described including x-ray, neutron and electron diffraction setups using modern day apparatus including synchrotron sources. Data corrections, essential for quantitative analysis are covered before the authors conclude with a discussion of the analysis methods themselves. The information is presented in a way that facilitates understanding the information content of the data, as well as best practices for collecting and analyzing data for quantitative analysis. This long awaited book condenses the knowledge of renowned experts in the field into a single, authoritative, overview of the application of powder diffraction in modern materials research. The book contains essential theory and introductory material for students and researchers wishing to learn how to apply the frontier methods of powder diffraction
| Author | : Angela Dibenedetto |
| Publisher | : Walter de Gruyter |
| Total Pages | : 232 |
| Release | : 2013-10-14 |
| Genre | : Science |
| ISBN | : 3110306875 |
The demand for new materials with novel properties on the micro- and nano-scale continues to grow. This book provides an overview of state-of-the-art techniques for the synthesis and characterization of inorganic nanomaterials including sonochemistry, microwave dielectric heating, sonoelectrochemistry and RAPET, high-throughput experimentation in heterogeneous catalyst research, photoluminescence, and methods for surface structuring. Imaging techniques include X-ray photoelectron spectroscopy, X-ray absorption spectroscopy, single crystal and powder X-ray diffraction, X-ray microimaging (SAXS,WAXS & GISAXS), electron microscopy, and solid state NMR. The work is essential reading for all researchers in academia and industry working in the field of nanosciences.
| Author | : Abraham Clearfield |
| Publisher | : |
| Total Pages | : 160 |
| Release | : 2002 |
| Genre | : Crystal engineering |
| ISBN | : |
| Author | : |
| Publisher | : |
| Total Pages | : 380 |
| Release | : 2007 |
| Genre | : Crystallography |
| ISBN | : |
| Author | : S. P. Sen Gupta |
| Publisher | : Allied Publishers |
| Total Pages | : 182 |
| Release | : 2002 |
| Genre | : Diffraction |
| ISBN | : 9788177642629 |
| Author | : Robert A. Scott |
| Publisher | : John Wiley & Sons |
| Total Pages | : 597 |
| Release | : 2007-12-10 |
| Genre | : Science |
| ISBN | : 0470032170 |
Modern spectroscopic and instrumental techniques are essential to the practice of inorganic and bioinorganic chemistry. This first volume in the new Wiley Encyclopedia of Inorganic Chemistry Methods and Applications Series provides a consistent and comprehensive description of the practical applicability of a large number of techniques to modern problems in inorganic and bioinorganic chemistry. The outcome is a text that provides invaluable guidance and advice for inorganic and bioinorganic chemists to select appropriate techniques, whilst acting as a source to the understanding of these methods. This volume is also available as part of Encyclopedia of Inorganic Chemistry, 5 Volume Set. This set combines all volumes published as EIC Books from 2007 to 2010, representing areas of key developments in the field of inorganic chemistry published in the Encyclopedia of Inorganic Chemistry. Find out more.
| Author | : Frank Smith |
| Publisher | : CRC Press |
| Total Pages | : 1026 |
| Release | : 1999-09-22 |
| Genre | : Science |
| ISBN | : 0824719921 |
By illustrating a wide range of specific applications in all major industries, this work broadens the coverage of X-ray diffraction beyond basic tenets, research and academic principles. The book serves as a guide to solving problems faced everyday in the laboratory, and offers a review of the current theory and practice of X-ray diffraction, major advances and potential uses.
