Spectrometric Identification Of Organic Compounds
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Author | : Robert Milton Silverstein |
Publisher | : |
Total Pages | : 0 |
Release | : 2005 |
Genre | : Organic compounds |
ISBN | : 9780471429135 |
Originally published in 1962, this was the first book to explore teh identification of organic compounds using spectroscopy. It provides a thorough introduction to the three areas of spectrometry most widely used in spectrometric identification: mass spectrometry, infrared spectrometry, and nuclear magnetic resonance spectrometry. A how-to, hands-on teaching manual with considerably expanded NMR coverage--NMR spectra can now be intrepreted in exquisite detail. This book: Uses a problem-solving approach with extensive reference charts and tables. Offers an extensive set of real-data problems offers a challenge to the practicing chemist
Author | : Ernö Pretsch |
Publisher | : Springer Science & Business Media |
Total Pages | : 444 |
Release | : 2000 |
Genre | : Science |
ISBN | : 9783540678151 |
Table -- Combination tables -- 13C NMR spectroscopy -- 1H NMR specroscopy -- IR spectroscopy -- Mass spectrometry -- UV/Vis spectroscopy.
Author | : Ernö Pretsch |
Publisher | : Springer Science & Business Media |
Total Pages | : 325 |
Release | : 2013-06-29 |
Genre | : Science |
ISBN | : 3662224550 |
Although numerical data are, in principle, universal, the compilations presented in this book are extensively annotated and interleaved with text. This translation of the second German edition has been prepared to facilitate the use of this work, with all its valuable detail, by the large community of English-speaking scientists. Translation has also provided an opportunity to correct and revise the text, and to update the nomenclature. Fortunately, spectroscopic data and their relationship with structure do not change much with time so one can predict that this book will, for a long period of time, continue to be very useful to organic chemists involved in the identification of organic compounds or the elucidation of their structure. Klaus Biemann Cambridge, MA, April 1983 Preface to the First German Edition Making use of the information provided by various spectroscopic tech niques has become a matter of routine for the analytically oriented organic chemist. Those who have graduated recently received extensive training in these techniques as part of the curriculum while their older colleagues learned to use these methods by necessity. One can, therefore, assume that chemists are well versed in the proper choice of the methods suitable for the solution of a particular problem and to translate the experimental data into structural information.
Author | : Karen Feinstein |
Publisher | : CRC Press |
Total Pages | : 140 |
Release | : 1994-11-22 |
Genre | : Science |
ISBN | : 9780849394485 |
Guide to Spectroscopic Identification of Organic Compounds is a practical "how-to" book with a general problem-solving algorithm for determining the structure of a molecule from complementary spectra or spectral data obtained from MS, IR, NMR, or UV spectrophotometers. Representative compounds are analyzed and examples are solved. Solutions are eclectic, ranging from simple and straightforward to complex. A picture of the relationship of structure to physical properties, as well as to spectral features, is provided. Compounds and their derivatives, structural isomers, straight-chain molecules, and aromatics illustrate predominant features exhibited by different functional groups. Practice problems are also included. Guide to Spectroscopic Identification of Organic Compounds is a helpful and convenient tool for the analyst in interpreting organic spectra. It may serve as a companion to any organic textbook or as a spectroscopy reference; its size allows practitioners to carry it along when other tools might be cumbersome or expensive.
Author | : Yong-Cheng Ning |
Publisher | : Wiley-VCH |
Total Pages | : 480 |
Release | : 2005-05-06 |
Genre | : Science |
ISBN | : |
Clearly structured, easy to read and optimal to understand, this extensive compendium fills the gap between textbooks devoted to either spectra interpretation or basic physical principles. The original Chinese editions have already sold over 18,500 copies, and the material is taken from the latest literature from around the world, plus technical information provided by the manufacturers of spectroscopic instruments. Alongside basic methods, Professor Ning presents up-to-date developments in NMR, MS, IR and Raman spectroscopy, such as pulsed-field gradient technique, LC-NMR, and DOSY. He stresses the application of spectroscopic methods, interpreting them in great detail and depth since most of the selected spectra may be applied to practical work, as well as summarizing the rules for their interpretation. He also incorporates his original ideas, including a comparison of the common points in different spectroscopic techniques. This monograph features a unique structure, a typical example being the discussion of 2D NMR starting from pulse sequence units, which construct various pulse sequences for related 2D NMR. A complete chapter deals with the determination of configurations and conformations of organic compounds and even biological molecules from the viewpoint of spectroscopic methodologies, while one whole section is dedicated to the interpretation of mass spectra produced by soft ionization techniques. The principles of mass analyzers, especially the ion trap, are discussed in great depth, together with a concise summary of the MS fragmentation and rearrangement of common compounds, allowing readers to easily predict related mass spectrometric reactions. All the three kinds of library retrieval of mass spectra are presented in detail, together with recent developments in molecular vibration spectroscopy. The whole is rounded off with several appendices, including a subject index for rapid reference. With a foreword by the Nobel prizewinner, Richard R. Ernst.
Author | : Robert B. Bates |
Publisher | : Springer Science & Business Media |
Total Pages | : 280 |
Release | : 2012-12-06 |
Genre | : Science |
ISBN | : 1461259959 |
With the advent of Fourier transform spectrometers of great sensitivity, it has become practical to obtain carbon-13 nuclear magnetic resonance (C-13 NMR; l3C NMR; CMR) spectra routinely on organic molecules, and this technique has become one of the highest utility in determining structures of organic unknowns. When the usual spectrometric techniques proton magnetic resonance (H-I NMR; IH NMR; PMR), infrared (lR), mass (MS), and ultraviolet (UV)-do not readily reveal a compound's structure, a C-13 NMR spectrum will often provide sufficient additional information to yield it unequivocally. With this in mind, the present work was designed to give advanced undergraduates, graduate students, and practicing chemists a working knowledge of and facility with the use of this valuable technique. Some familiarity with other spectrometric techniques is assumed (recommended book: Silverstein, Bassler, and Morrill, Spectrometric Identification of Organic Compounds), but no prior knowledge of C-13 NMR -which is treated very lightly, if at all, in the widely used elementary organic texts-is necessary. A discussion of C-13 NMR spectroscopy is followed by 125 problems, each consisting of a molecular formula, two types of C-13 NMR spectra (partially and completely proton decoupled, with connecting lines to facilitate multiplicity assignments), an integrated H-I NMR spectrum, and the most important IR, UV, and MS data. These problems have been very carefully prepared, thoroughly tested by students at the University of Arizona, and we believe that very few errors remain.
Author | : Dudley H. Williams |
Publisher | : McGraw-Hill Companies |
Total Pages | : 268 |
Release | : 1980 |
Genre | : Science |
ISBN | : |
Author | : L. D. Field |
Publisher | : |
Total Pages | : 304 |
Release | : 1995-12-26 |
Genre | : Science |
ISBN | : |
Offers a realistic approach to solving problems used by organic chemists. Covering all the major spectroscopic techniques, it provides a graded set of problems that develop and consolidate students' understanding of organic spectroscopy. This edition contains more elementary problems and a modern approach to NMR spectra.
Author | : Phillip Crews |
Publisher | : |
Total Pages | : 664 |
Release | : 2010 |
Genre | : Medical |
ISBN | : |
"Organic Structure Analysis, Second Edition, is the only text that teaches students how to solve structures as they are solved in actual practice. Ideal for advanced undergraduate and graduate courses in organic structure analysis, organic structure identification, and organic spectroscopy, it emphasizes real applications-integrating theory as needed - and introduces students to the latest spectroscopic methods." --Book Jacket.
Author | : Jeffrey H. Simpson |
Publisher | : Academic Press |
Total Pages | : 591 |
Release | : 2011-12-30 |
Genre | : Science |
ISBN | : 0123849705 |
"The second edition of this book comes with a number of new figures, passages, and problems. Increasing the number of figures from 290 to 448 has necessarily added considerable length, weight, and, expense. It is my hope that the book has not lost any of its readability and accessibility. I firmly believe that most of the concepts needed to learn organic structure determination using nuclear magnetic resonance spectroscopy do not require an extensive mathematical background. It is my hope that the manner in which the material contained in this book is presented both reflects and validates this belief"--