Sampling For Analytical Purposes
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| Author | : Pierre Gy |
| Publisher | : John Wiley & Sons |
| Total Pages | : 180 |
| Release | : 1998-06-29 |
| Genre | : Science |
| ISBN | : 9780471979562 |
Dr Gy, a pioneer in every sense of the word, has spent 50 years studying the best way to take a truly representative sample. His greatest achievement perhaps has been to introduce science into the black art of sampling. The now famous and widely used formula bearing his name means that sampling is no longer a lottery but an essential analytical tool. This very readable and practical book, written by Pierre Gy himself, is the first simple guide to Pierre Gy s method to be translated into English. Although Dr Gy s formula was originally developed for the sampling of solid material in mines, etc., the theoretical arguments are equally valid for the sampling of liquids and multi-phase media. This book is as interesting as a historical perspective as it is useful for the practising modern day analyst.
| Author | : Josep M. Bayona |
| Publisher | : Academic Press |
| Total Pages | : 2998 |
| Release | : 2012-12-31 |
| Genre | : Science |
| ISBN | : 0123813743 |
Comprehensive Sampling and Sample Preparation is a complete treatment of the theory and methodology of sampling in all physical phases and the theory of sample preparation for all major extraction techniques. It is the perfect starting point for researchers and students to design and implement their experiments and support those experiments with quality-reviewed background information. In its four volumes, fundamentals of sampling and sample preparation are reinforced through broad and detailed sections dealing with Biological and Medical, Environmental and Forensic, and Food and Beverage applications. The contributions are organized to reflect the way in which analytical chemists approach a problem. It is intended for a broad audience of analytical chemists, both educators and practitioners of the art and can assist in the preparation of courses as well in the selection of sampling and sample preparation techniques to address the challenges at hand. Above all, it is designed to be helpful in learning more about these topics, as well as to encourage an interest in sampling and sample preparation by outlining the present practice of the technology and by indicating research opportunities. Sampling and Sample preparation is a large and well-defined field in Analytical Chemistry, relevant for many application areas such as medicine, environmental science, biochemistry, pharmacology, geology, and food science. This work covers all these aspects and will be extremely useful to researchers and students, who can use it as a starting point to design and implement their experiments and for quality-reviewed background information There are limited resources that Educators can use to effectively teach the fundamental aspects of modern sample preparation technology. Comprehensive Sampling and Sample Preparation addresses this need, but focuses on the common principles of new developments in extraction technologies rather than the differences between techniques thus facilitating a more thorough understanding Provides a complete overview of the field. Not only will help to save time, it will also help to make correct assessments and avoid costly mistakes in sampling in the process Sample and sample preparation are integral parts of the analytical process but are often less considered and sometimes even completely disregarded in the available literature. To fill this gap, leading scientists have contributed 130 chapters, organized in 4 volumes, covering all modern aspects of sampling and liquid, solid phase and membrane extractions, as well as the challenges associated with different types of matrices in relevant application areas
| Author | : Rafael Lucena |
| Publisher | : Elsevier |
| Total Pages | : 573 |
| Release | : 2021-10-23 |
| Genre | : Science |
| ISBN | : 0128221720 |
Analytical Sample Preparation With Nano- and Other High-Performance Materials covers advanced sample treatment techniques and the new materials that can be used to boost their performance. The evolution of sample treatment over the last two decades has resulted in the development of new techniques and application of new materials. This is a must-have resource for those studying advanced analytical techniques and the role of high-performance materials in analytical chemistry. The book explains the underlying principles needed to properly understand sample preparation, and also examines the latest materials - including nanomaterials - that result in greater sensitivity and specificity. The book begins with a section devoted to all the various sample preparation techniques and then continues with sections on high-performance sorbents and high-performance solvents. - Combines basic, fundamental principles and advanced concepts and applications for a comprehensive treatment of sample preparation with new materials - Defines nano- and other high-performance materials in this context, including carbon nanoparticles, inorganic nanoparticles, ionic liquids, supramolecular solvents, and more - Includes discussion of all the latest advancements and new findings in both techniques and materials used for proper sample preparation
| Author | : Maria Elayna Mosley |
| Publisher | : Cornell University Press |
| Total Pages | : 313 |
| Release | : 2013-05-15 |
| Genre | : Political Science |
| ISBN | : 0801467969 |
Interviews are a frequent and important part of empirical research in political science, but graduate programs rarely offer discipline-specific training in selecting interviewees, conducting interviews, and using the data thus collected. Interview Research in Political Science addresses this vital need, offering hard-won advice for both graduate students and faculty members. The contributors to this book have worked in a variety of field locations and settings and have interviewed a wide array of informants, from government officials to members of rebel movements and victims of wartime violence, from lobbyists and corporate executives to workers and trade unionists. The authors encourage scholars from all subfields of political science to use interviews in their research, and they provide a set of lessons and tools for doing so. The book addresses how to construct a sample of interviewees; how to collect and report interview data; and how to address ethical considerations and the Institutional Review Board process. Other chapters discuss how to link interview-based evidence with causal claims; how to use proxy interviews or an interpreter to improve access; and how to structure interview questions. A useful appendix contains examples of consent documents, semistructured interview prompts, and interview protocols.
| Author | : Chunlong Zhang |
| Publisher | : John Wiley & Sons |
| Total Pages | : 458 |
| Release | : 2007-02-26 |
| Genre | : Science |
| ISBN | : 0470120673 |
An integrated approach to understanding the principles of sampling, chemical analysis, and instrumentation This unique reference focuses on the overall framework and why various methodologies are used in environmental sampling and analysis. An understanding of the underlying theories and principles empowers environmental professionals to select and adapt the proper sampling and analytical protocols for specific contaminants as well as for specific project applications. Covering both field sampling and laboratory analysis, Fundamentals of Environmental Sampling and Analysis includes: A review of the basic analytical and organic chemistry, statistics, hydrogeology, and environmental regulations relevant to sampling and analysis An overview of the fundamentals of environmental sampling design, sampling techniques, and quality assurance/quality control (QA/QC) essential to acquire quality environmental data A detailed discussion of: the theories of absorption spectroscopy for qualitative and quantitative environmental analysis; metal analysis using various atomic absorption and emission spectrometric methods; and the instrumental principles of common chromatographic and electrochemical methods An introduction to advanced analytical techniques, including various hyphenated mass spectrometries and nuclear magnetic resonance spectroscopy With real-life case studies that illustrate the principles plus problems and questions at the end of each chapter to solidify understanding, this is a practical, hands-on reference for practitioners and a great textbook for upper-level undergraduates and graduate students in environmental science and engineering.
| Author | : E. P. Popek |
| Publisher | : Academic Press |
| Total Pages | : 378 |
| Release | : 2003-07-08 |
| Genre | : Language Arts & Disciplines |
| ISBN | : 9780125615402 |
An excellent introduction to the real world of environmental work, this book covers all phases of data collection, (planning, field sampling, laboratory analysis, and data quality assessment), and is a single source comprehensive reference for the resolution of the most common problems that environmental professionals face daily in their work. (Midwest).
| Author | : Janusz Pawliszyn |
| Publisher | : Elsevier |
| Total Pages | : 1170 |
| Release | : 2002-09-09 |
| Genre | : Science |
| ISBN | : 9780444505101 |
This title is the first comprehensive book on sampling and modern sample preparation techniques and has several main objectives: to facilitate recognition of sample preparation as both an integral part of the analytical process; to present a fundamental basis and unified theoretical approach for the professional development of sample preparation; to emphasize new developments in sample preparation technology; and to highlight the future impact of sample preparation on new directions in analytical science, particularly automation, miniaturization and field implementation. Until recently, there has been relatively little scientific interest in sampling and sample preparation, however this situation is presently changing as sampling and sample preparation become integral parts of the analytical process with their own unique challenges and research opportunities. Sampling and Sample Preparation for Field and Laboratory is an essential resource for all analytical chemists, and in particular those involved in method development. Not only does it cover the fundamental aspects of extraction, it also covers applications in various matrices and includes sampling strategies and equipment and how these can be integrated into the analytical process for maximum efficiency.
| Author | : Sharon L. Lohr |
| Publisher | : CRC Press |
| Total Pages | : 923 |
| Release | : 2019-04-08 |
| Genre | : Mathematics |
| ISBN | : 1000022544 |
This edition is a reprint of the second edition published by Cengage Learning, Inc. Reprinted with permission. What is the unemployment rate? How many adults have high blood pressure? What is the total area of land planted with soybeans? Sampling: Design and Analysis tells you how to design and analyze surveys to answer these and other questions. This authoritative text, used as a standard reference by numerous survey organizations, teaches sampling using real data sets from social sciences, public opinion research, medicine, public health, economics, agriculture, ecology, and other fields. The book is accessible to students from a wide range of statistical backgrounds. By appropriate choice of sections, it can be used for a graduate class for statistics students or for a class with students from business, sociology, psychology, or biology. Readers should be familiar with concepts from an introductory statistics class including linear regression; optional sections contain the statistical theory, for readers who have studied mathematical statistics. Distinctive features include: More than 450 exercises. In each chapter, Introductory Exercises develop skills, Working with Data Exercises give practice with data from surveys, Working with Theory Exercises allow students to investigate statistical properties of estimators, and Projects and Activities Exercises integrate concepts. A solutions manual is available. An emphasis on survey design. Coverage of simple random, stratified, and cluster sampling; ratio estimation; constructing survey weights; jackknife and bootstrap; nonresponse; chi-squared tests and regression analysis. Graphing data from surveys. Computer code using SAS® software. Online supplements containing data sets, computer programs, and additional material. Sharon Lohr, the author of Measuring Crime: Behind the Statistics, has published widely about survey sampling and statistical methods for education, public policy, law, and crime. She has been recognized as Fellow of the American Statistical Association, elected member of the International Statistical Institute, and recipient of the Gertrude M. Cox Statistics Award and the Deming Lecturer Award. Formerly Dean’s Distinguished Professor of Statistics at Arizona State University and a Vice President at Westat, she is now a freelance statistical consultant and writer. Visit her website at www.sharonlohr.com.
| Author | : Jaroslava Švarc-Gajić |
| Publisher | : |
| Total Pages | : 0 |
| Release | : 2012 |
| Genre | : Analytical chemistry |
| ISBN | : 9781621002697 |
The art of sample manipulation considers adequate sample collection, preservation and storage, as well as its safe preparation. Analytical chemists often find themselves in a position to spend considerable more time and effort in preparing samples rather than analysing them. In many cases the reliability of analysis is limited by the correctness of sample manipulation. The skills of sample manipulation are based on abundant knowledge, competence and rich experience. Being indispensable in every laboratory, educational or scientific institution, this book encompasses all relevant issues related to collecting samples of any kind, as well as methods of sample preparation for specific analytical goal. The presented material provides an overview of sampling principles and strategies supporting them with inevitable statistical background.
| Author | : Peter Bedson |
| Publisher | : Royal Society of Chemistry |
| Total Pages | : 401 |
| Release | : 2021-04-08 |
| Genre | : Mathematics |
| ISBN | : 1839164433 |
Analytical chemists must use a range of statistical tools in their treatment of experimental data to obtain reliable results. Practical Statistics for the Analytical Scientist is a manual designed to help them negotiate the daunting specialist terminology and symbols. Prepared in conjunction with the Department of Trade and Industry's Valid Analytical Measurement (VAM) programme, this volume covers the basic statistics needed in the laboratory. It describes the statistical procedures that are most likely to be required including summary and descriptive statistics, calibration, outlier testing, analysis of variance and basic quality control procedures. To improve understanding, many examples provide the user with material for consolidation and practice. The fully worked answers are given both to check the correct application of the procedures and to provide a template for future problems. Practical Statistics for the Analytical Scientist will be welcomed by practising analytical chemists as an important reference for day to day statistics in analytical chemistry.
