Pyrolysis Gas Chromatography Mass Spectrometry Of Polymeric Materials Second Edition
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| Author | : Shin Tsuge |
| Publisher | : Elsevier |
| Total Pages | : 405 |
| Release | : 2011-08-02 |
| Genre | : Science |
| ISBN | : 0444538933 |
In this data book, both conventional Py-GC/MS where thermal energy alone is used to cause fragmentation of given polymeric materials and reactive Py-GC/MS in the presence of organic alkaline for condensation polymers are compiled. Before going into detailed presentation of the data, however, acquiring a firm grip on the proper understanding about the situation of Py-GC/MS would promote better utilization of the following pyrolysis data for various polymers samples. This book incorporates recent technological advances in analytical pyrolysis methods especially useful for the characterization of 163 typical synthetic polymers. The book briefly reviews the instrumentation available in advanced analytical pyrolysis, and offers guidance to perform effectually this technique combining with gas chromatography and mass spectrometry. Main contents are comprehensive sample pyrograms, thermograms, identification tables, and representative mass spectra (MS) of pyrolyzates for synthetic polymers. This edition also highlights thermally-assisted hydrolysis and methylation technique effectively applied to 33 basic condensation polymers. - Coverage of Py-GC/MS data of conventional pyrograms and thermograms of basic 163 kinds of synthetic polymers together with MS and retention index data for pyrolyzates, enabling a quick identification - Additional coverage of the pyrograms and their related data for 33 basic condensation polymers obtained by the thermally-assisted hydrolysis and methylation technique - All compiled data measured under the same experimental conditions for pyrolysis, gas chromatography and mass spectrometry to facilitate peak identification - Surveyable instant information on two facing pages dedicated to the whole data of a given polymer sample
| Author | : Peter Kusch |
| Publisher | : World Scientific |
| Total Pages | : 267 |
| Release | : 2018-10-08 |
| Genre | : Science |
| ISBN | : 1786345773 |
The methodology of analytical pyrolysis-GC/MS has been known for several years, but is seldom used in research laboratories and process control in the chemical industry. This is due to the relative difficulty of interpreting the identified pyrolysis products as well as the variety of them. This book contains full identification of several classes of polymers/copolymers and biopolymers that can be very helpful to the user. In addition, the practical applications can encourage analytical chemists and engineers to use the techniques explored in this volume.The structure and the functions of various types of pyrolyzers and the results of the pyrolysis-gas chromatographic-mass spectrometric identification of synthetic polymers/copolymers and biopolymers at 700°C are described. Practical applications of these techniques are also included, detailing the analysis of microplastics, failure analysis in the automotive industry and solutions for technological problems.
| Author | : Peter Kusch |
| Publisher | : World Scientific |
| Total Pages | : 383 |
| Release | : 2023-08-28 |
| Genre | : Science |
| ISBN | : 1800613008 |
Readers will find many practical applications of pyrolysis-GC/MS as well as R&D usage in this newly revised and expanded edition. Detailed experimental descriptions for the identification of synthetic polymers and copolymers are included. This volume presents the current state of analytical pyrolysis, and contains full identification of several classes of polymers/copolymers and biopolymers that readers will find helpful. Structures and functions of various types of pyrolyzers are explored, as well as the results of the pyrolysis-gas chromatographic-mass spectrometric identification of synthetic polymers/copolymers and biopolymers at 700°C.Practical applications of this hyphenated technique, detailing the analysis of microplastics, failure analysis in the automotive industry and solutions for technological problems are provided. Numerous practical applications of pyrolysis-GC/MS, for industrial and R&D usage, will be of benefit to Chemists and Engineers, as well as for students of Chemistry and Polymer Sciences.
| Author | : James Robertson |
| Publisher | : CRC Press |
| Total Pages | : 470 |
| Release | : 2002-09-11 |
| Genre | : Law |
| ISBN | : 0203484517 |
This book is the definitive text for forensic scientists, police and lawyers who may be involved with the use of textile fibres to provide evidence in criminal cases. While covering the subject in detail from recovery of the evidence, through the different stages of laboratory examination, to evaulating the meaning of findings, it is written in such a way that it should be interesting and understandable to the beginner and to the layman, as well as to the expert.
| Author | : Michael Bolgar |
| Publisher | : CRC Press |
| Total Pages | : 626 |
| Release | : 2015-09-25 |
| Genre | : Science |
| ISBN | : 1439860750 |
Polymers have undoubtedly changed the world through many products that improve our lives. However, additives used to modify the overall characteristics of these materials may not be fully disclosed or understood. These additives may present possible environmental and health hazards. It is important to monitor consumer products for these compounds u
| Author | : Giorgio Montaudo |
| Publisher | : CRC Press |
| Total Pages | : 601 |
| Release | : 2001-10-29 |
| Genre | : Science |
| ISBN | : 1420037757 |
Mass Spectrometry (MS) has rapidly become an indispensable tool in polymer analysis, and modern MS today complements in many ways the structural data provided by Nuclear Magnetic Resonance (NMR) and Infrared (IR) methods. Recent advances have sparked a growing interest in this field and established a need for a summary of progress made and results
| Author | : Jehane Ragai |
| Publisher | : World Scientific |
| Total Pages | : 274 |
| Release | : 2018-01-31 |
| Genre | : Art |
| ISBN | : 178634422X |
In The Scientist and the Forger: Probing a Turbulent Art World the author draws upon an enthralling range of case studies, from Botticelli to Leonardo, Campendonk to Pollock and Chagall to Freud, equipping the reader with a holistic understanding of an art world shaped by fast-moving trends, and increasingly permeated by science. We are taken on a gripping journey, becoming witness to the attempts currently being made to safeguard a partly complicit art market virtually under siege.How can we determine whether it was Leonardo's hand that created Salvator Mundi? How can we prove that a suspected Pollock is a forgery? And how can Man in a Black Cravat be seemingly incontrovertibly attributed to Lucian Freud, despite this artist's adamant refusal to recognize it as one of his own? This book reveals how art historians and scientists collaborate conclusively to authenticate paintings or demonstrate that they are forgeries, and as the enigma of La Bella Principessa continues to baffle, the question remains: do we have enough reason to hope that we shall one day know her true story? Building on the first edition, a more in depth look is taken at some of the greatest scandals to date — with an interpretation of the psychological behavior of Ann Freedman the former president and director of the Knoedler Gallery.
| Author | : S.C. Moldoveanu |
| Publisher | : Elsevier |
| Total Pages | : 949 |
| Release | : 2002-05-08 |
| Genre | : Science |
| ISBN | : 0080540708 |
Sample preparation is an essential step in many analyses. This book approaches the topic of sample preparation in chromatography in a methodical way, viewing it as a logical connection between sample collection and analytical chromatography. Providing a guide for choosing the appropriate sample preparation for a given analysis, this book describes various ways to process the sample, explaining the principle, discussing the advantages and disadvantages, describing the applicability to different types of samples, and showing the fitness to specific chromatographic determinations. The first part of the book contains an overview of sample preparation showing its relation to sample collection and to the core chromatographic analysis. The second part covers procedures that do not use chemical modifications of the analyte and includes methods for sample dissolution, concentration and cleanup designed mainly for modifying the initial matrix of the sample. This part starts with conventional separations such as filtration and distillation and finishes with more advanced techniques such as solid phase extraction and electroseparations. The third part gives a description of the chemical modifications that can be performed on a sample either for fractionation purposes or to improve a specific property of the analyte. This part includes derivatizations, polymer chemical degradations, and pyrolysis.
| Author | : Serban C. Moldoveanu |
| Publisher | : Elsevier |
| Total Pages | : 714 |
| Release | : 2005-01-20 |
| Genre | : Science |
| ISBN | : 0080455867 |
Analytical Pyrolysis of Synthetic Organic Polymers is a follow-up to Analytical Pyrolysis of Natural Organic Polymers, which is volume 20 of the series. The main focus of the book is on practical applications of analytical pyrolysis in synthetic organic polymer identification and characterization. The first part of the book has five chapters including an introduction, a discussion on physico-chemistry of thermal degradation of synthetic polymers and on instrumentation used in analytical pyrolysis, a chapter discussing what type of information can be obtained from analytical pyrolysis, and a chapter dedicated to the analysis and characterization of synthetic polymers.The second part systematically covers the analytical pyrolysis of various classes of synthetic polymers. Some theoretical background for the understanding of polymer structure using analytical pyrolysis is also discussed.* Includes broad coverage of organic synthetic macromolecules* Focuses on physico-chemistry of thermal degradation, and the analytical pyrolysis of various classes of synthetic polymers* Is well written and suitable for both researchers and chemists working in analytical chemistry or in synthetic polymers
| Author | : Mustafa Ali Mohd |
| Publisher | : BoD – Books on Demand |
| Total Pages | : 474 |
| Release | : 2012-03-21 |
| Genre | : Science |
| ISBN | : 9535102982 |
Progress in agricultural, biomedical and industrial applications' is a compilation of recent advances and developments in gas chromatography and its applications. The chapters cover various aspects of applications ranging from basic biological, biomedical applications to industrial applications. Book chapters analyze new developments in chromatographic columns, microextraction techniques, derivatisation techniques and pyrolysis techniques. The book also includes several aspects of basic chromatography techniques and is suitable for both young and advanced chromatographers. It includes some new developments in chromatography such as multidimensional chromatography, inverse chromatography and some discussions on two-dimensional chromatography. The topics covered include analysis of volatiles, toxicants, indoor air, petroleum hydrocarbons, organometallic compounds and natural products. The chapters were written by experts from various fields and clearly assisted by simple diagrams and tables. This book is highly recommended for chemists as well as non-chemists working in gas chromatography.
