Overview of On-site Analytical Methods for Explosives in Soil

Overview of On-site Analytical Methods for Explosives in Soil
Author:
Publisher:
Total Pages: 74
Release: 1998
Genre: Explosives
ISBN:

The purpose of this report is to survey the current status of field sampling and on-site analytical methods for detecting and quantifying secondary explosives compounds in soils (Table 1). The paper also includes a brief discussion of EPA Method 8330 (EPA 1995), the reference analytical method for the determination of 14 explosives and co-contaminants in soil. This report is divided into the following major sections: introduction; background; an overview of sampling and analysis for explosives in soil; data quality objectives; unique sampling design considerations for explosives; procedures for statistically comparing on-site and reference analytical methods; a summary of on-site analytical methods; and a summary of the current EPA reference analytical method, Method 8330 (EPA 1995). Although some sections may be used independently, joint use of the field sampling and on-site analytical methods sections is recommended to develop a sampling and analytical approach that achieves project objectives.

Aspects of Explosives Detection

Aspects of Explosives Detection
Author: Maurice Marshall
Publisher: Elsevier
Total Pages: 303
Release: 2011-07-28
Genre: Science
ISBN: 0080923143

Detection and quantification of trace chemicals is a major thrust of analytical chemistry. In recent years much effort has been spent developing detection systems for priority pollutants. Less mature are the detections of substances of interest to law enforcement and security personnel:in particular explosives. This volume will discuss the detection of these, not only setting out the theoretical fundamentals, but also emphasizing the remarkable developments in the last decade. Terrorist events—airplanes blown out of the sky (PanAm 103 over Lockerbie) and attacks on U.S. and European cities (Trade Center in New York and the Murrah Federal Building in Oklahoma City, railways in London and Madrid)--emphasize the danger of concealed explosives. However, since most explosives release little vapor, it was not possible to detect them by technology used on most organic substances. After PanAm 103 was downed over Scotland, the U.S. Congress requested automatic explosive detection equipment be placed in airports. This volume outlines the history of explosive detection research, the developments along the way, present day technologies, and what we think the future holds. - Written by experts in the field who set out both the scientific issues and the practical context with authority - Discusses and describes the threat - Describes the theoretical background and practical applications of both trace and bulk explosives detection

Field Gas Chromatography/thermionic Detector System for On-site Determination of Explosives in Soils

Field Gas Chromatography/thermionic Detector System for On-site Determination of Explosives in Soils
Author: Alan Dole Hewitt
Publisher:
Total Pages: 32
Release: 2001
Genre: Explosives
ISBN:

On-site determination of nitroaromatic, nitramine, and nitrate ester explosives compounds in soils was performed using a field-portable gas chromatograph (GC)equipped with a thermionic ionization detector (TID)selective for compounds with nitro functional groups. Soil samples were extracted with acetone. A 1 microliter volume of the filtered soil extract was manually injected into the GC, allowing for the rapid qualification and quantification of the suite of explosives that often coexist in soils at military training facilities and other defense-related sites. Good agreement was established for the concentrations of several explosives analytes when this method of analysis was compared to either high-performance liquid chromatography (Method 8330)or GC electron capture (Method 8095)analysis. Comparisons were performed for sample extracts and for soil subsample replicates distributed for on-site preparation and analysis during a field verification test performed under the auspices of the U.S. Environmental Protection Agency's Environmental Technology Verification (ETV)Program.

Forensic Investigation of Explosions

Forensic Investigation of Explosions
Author: Alexander Beveridge
Publisher: CRC Press
Total Pages: 818
Release: 2011-11-02
Genre: Law
ISBN: 1420087266

Now in its second edition, Forensic Investigation of Explosions draws on the editor‘s 30 years of explosives casework experience, including his work on task forces set up to investigate major explosives incidents. Dr. Alexander Beveridge provides a broad, multidisciplinary approach, assembling the contributions of internationally recognized experts