Materials Characterization By Dynamic And Modulated Thermal Analytical Techniques
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| Author | : Alan T. Riga |
| Publisher | : ASTM International |
| Total Pages | : 216 |
| Release | : 2001 |
| Genre | : Calorimetry |
| ISBN | : 0803128878 |
The special technical publication has been compiled from the 15 presentations at a May 2000 Association symposium in Toronto. They cover the fundamentals of the techniques, its use in curing and chemical reactions, measuring the glass transition and melting by modulated and comparative techniques, g
| Author | : Kevin P. Menard |
| Publisher | : CRC Press |
| Total Pages | : 281 |
| Release | : 2020-05-04 |
| Genre | : Science |
| ISBN | : 1482255529 |
Dynamic Mechanical Analysis (DMA) is a powerful technique for understanding the viscoelastic properties of materials. It has become a powerful tool for chemists, polymer and material scientists, and engineers. Despite this, it often remains underutilized in the modern laboratory. Because of its high sensitivity to the presence of the glass transition, many users limit it to detecting glass transitions that can’t be seen by differential scanning calorimetry (DSC). This book presents a practical and straightforward approach to understanding how DMA works and what it measures. Starting with the concepts of stress and strain, the text takes the reader through stress–strain, creep, and thermomechanical analysis. DMA is discussed as both the instrument and fixtures as well as the techniques for measuring both thermoplastic and thermosetting behavior. This edition offers expanded chapters on these areas as well as frequency scanning and other application areas. To help the reader grasp the material, study questions have also been added. Endnotes have been expanded and updated. Features Reflects the latest DMA research and technical advances Includes case studies to demonstrate the use of DMA over a range of industrial problems Includes numerous references to help those with limited materials engineering background Demonstrates the power of DMA as a laboratory tool for analysis and testing
| Author | : Joseph D. Menczel |
| Publisher | : John Wiley & Sons |
| Total Pages | : 607 |
| Release | : 2014-07-09 |
| Genre | : Science |
| ISBN | : 1118995996 |
Presents a solid introduction to thermal analysis, methods, instrumentation, calibration, and application along with the necessary theoretical background. Useful to chemists, physicists, materials scientists, and engineers who are new to thermal analysis techniques, and to existing users of thermal analysis who wish expand their experience to new techniques and applications Topics covered include Differential Scanning Calorimetry and Differential Thermal Analysis (DSC/DTA), Thermogravimetry, Thermomechanical Analysis and Dilatometry, Dynamic Mechanical Analysis, Micro-Thermal Analysis, Hot Stage Microscopy, and Instrumentation. Written by experts in the various areas of thermal analysis Relevant and detailed experiments and examples follow each chapter.
| Author | : Ch Sateesh Kumar |
| Publisher | : CRC Press |
| Total Pages | : 145 |
| Release | : 2023-05-04 |
| Genre | : Technology & Engineering |
| ISBN | : 1000872297 |
The book covers various methods of characterization of advanced materials commonly used in engineering including understanding of the working principle and applicability of devices. It explores the techniques implemented for advanced materials like superalloys, thin films, powders, nanocomposites, polymers, shape memory alloys, high entropy alloys, and so on. Major instruments covered include X-ray diffraction, near-field scanning optical microscopy Raman, X-ray photospectroscopy, ultraviolet-visible-near-infrared spectrosphotometer, Fourier-transform infrared spectroscopy, differential scanning calorimeter, profilometer, and thermogravimetric analysis. Features: Covers material characterization techniques and the development of advanced characterization technology Includes multiple length scale characterization approaches for a large variety of materials, from nano- to micron-scale, as well as their constraints Discusses advanced material characterization technology in the microstructural and property characterization fields Reviews both practical and theoretical explanations of approaches for characterizing microstructure and properties Offers fundamentals, basic instrumentation details, experimental approaches, analyses, and applications with case studies This book is aimed at graduate students and researchers in materials science and engineering.
| Author | : El-Zeiny Ebeid |
| Publisher | : Elsevier |
| Total Pages | : 324 |
| Release | : 2021-06-23 |
| Genre | : Science |
| ISBN | : 0323901921 |
Thermal Analysis: From Introductory Fundamentals to Advanced Applications presents an easy-to-understand introduction to Thermal Analysis (TA) principles alongside in-depth coverage of the wide variety of techniques currently in use across several industries. It covers differential scanning calorimetry (DSC), temperature modulated DSC (TMDSC), differential thermal analysis (DTA), thermogravimetry (TG) or thermogravimetric analysis (TGA), thermomechanical analysis (TMA), differential photo-calorimetry (DPC), dynamic mechanical analysis (DMA), thermodilatometry (TD), dielectric thermal analysis (DEA), thermally-stimulated current (TSC), emanation thermal analysis (ETA), thermoluminescence (TL), fast scanning calorimetry (FSC), and microcalorimetry. Chapters define the various TA techniques, report the Temperature-Modulated DSC (TMDSC) method and its applications, especially its use for studying the thermodynamic properties of polymers and pharmaceuticals, focus on the potential of TA in materials science with applications in chemistry and engineering, demonstrate, in detail, the various applications of TA in food, electronic industries, solid-state reactions, chemistry of polymers and large directing agents, kinetic studies, demonstrate the crystal structure and phase changes occurring upon heating by TA, and the potential of TA in recycling and waste management. - Gives a solid introduction to the scientific principles of TA for those who are new to these techniques or need a deeper understanding - Illustrates concepts with more than 100 schematic and analysis curves, several flow charts, process diagrams and photographs - Contains chapters that cover the user of TA in materials science and crystal structures
| Author | : Duncan Q.M. Craig |
| Publisher | : CRC Press |
| Total Pages | : 416 |
| Release | : 2006-12-21 |
| Genre | : Medical |
| ISBN | : 1420014897 |
As a result of the Process Analytical Technologies (PAT) initiative launched by the U.S. Food and Drug Administration (FDA), analytical development is receiving more attention within the pharmaceutical industry. Illustrating the importance of analytical methodologies, Thermal Analysis of Pharmaceuticals presents reliable and versatile charac
| Author | : Hubert Lobo |
| Publisher | : CRC Press |
| Total Pages | : 656 |
| Release | : 2003-06-25 |
| Genre | : Science |
| ISBN | : 0203911989 |
Plastics possess properties that have revolutionized the manufacture of products in the 20th century and beyond. It remains critical to understand their behavior throughout their life cycle, from manufacture to use and eventually to reclamation and disposal. This volume highlights the most prominent tools in physical and chemical analysis techniques and applications. A practical reference for performing measurements, solving problems, and investigating behavioral phenomena, the editors advocate a phenomenological approach, relying on case studies and illustrations to represent possible outcomes of each technique and presenting the basic governing equations where necessary.
| Author | : Piervincenzo Rizzo |
| Publisher | : Springer Nature |
| Total Pages | : 1078 |
| Release | : 2022-06-21 |
| Genre | : Technology & Engineering |
| ISBN | : 3031073223 |
This volume gathers the latest advances, innovations, and applications in the field of structural health monitoring (SHM) and more broadly in the fields of smart materials and intelligent systems, as presented by leading international researchers and engineers at the 10th European Workshop on Structural Health Monitoring (EWSHM), held in Palermo, Italy on July 4-7, 2022. The volume covers highly diverse topics, including signal processing, smart sensors, autonomous systems, remote sensing and support, UAV platforms for SHM, Internet of Things, Industry 4.0, and SHM for civil structures and infrastructures. The contributions, which are published after a rigorous international peer-review process, highlight numerous exciting ideas that will spur novel research directions and foster multidisciplinary collaboration among different specialists.
| Author | : Miriam Schuster |
| Publisher | : Springer Nature |
| Total Pages | : 356 |
| Release | : 2022-12-21 |
| Genre | : Technology & Engineering |
| ISBN | : 3658398213 |
Laminated safety glass enables the safe construction of transparent structures. The mechanical behaviour depends on the polymeric interlayer both in the intact and in the post fracture state. In the present work, the mechanical behaviour of ethylene vinyl acetate-based (EVA) and ionoplastic interlayers is investigated for the intact laminated safety glass condition. In particular, the influence of the semi-crystalline structure on the stiffness behaviour is studied with X-Ray Diffraction, Differential Scanning Calorimetry and Dynamic-Mechanical-Thermal-Analysis. The studies on the mechanical behaviour of the interlayer in the fractured laminated safety glass were carried out with polyvinyl butyral-based (PVB) interlayers. First, the temperature and frequency (time) dependent linearity limits are determined in Dynamic-Mechanical-Thermal-Analyses, second, the nonlinear viscoelastic material behaviour is investigated with tensile relaxation tests at different temperatures and strain levels.
| Author | : Mike Jenkins |
| Publisher | : Elsevier |
| Total Pages | : 293 |
| Release | : 2012-08-13 |
| Genre | : Medical |
| ISBN | : 0857096516 |
Given the widespread use of polymers in medical devices, the durability and reliability of this material in use is an area of critical importance. Durability and reliability of medical polymers reviews the performance of both bioresorbable and non-bioresorbable medical polymers.Part one provides a review of the types and properties of bioresorbable medical polymers. The effect of molecular structure on properties is discussed, along with the processing of bioresorbable and other polymers for medical applications. Transport phenomena and the degradation of bioresorbable medical polymers are reviewed, before an exploration of synthetic bioresorbable polymers and their use in orthopaedic tissue regeneration. Part two goes on to explore the durability and reliability of non-bioresorbable medical polymers, and wear processes in polymer implants and ageing processes of biomedical polymers in the body are discussed in depth, before an investigation into manufacturing defects and the failure of synthetic polymeric medical devices.With its distinguished editors and international team of expert contributors, Durability and reliability of medical polymers is an essential tool for all materials scientists, researchers and engineers involved in the design, development and application of medical polymers, whilst also providing a helpful overview of the subject for biologists, chemist and clinicians. - Comprehensively examines the performance of both bioresorbable and non-bioresorbable medical polymers - Discusses the processing of bioresorbable and other polymers for medical applications, before reviewing the degradation of bioresorbable medical polymers - Explores the durability and reliability of non-bioresorbable medical polymers and discusses wear processes in polymer implants and ageing processes of biomedical polymers in the body
