Quality Assurance for Environmental Analysis

Quality Assurance for Environmental Analysis
Author: E.A. Maier
Publisher: Elsevier
Total Pages: 670
Release: 1995-01-13
Genre: Science
ISBN: 0080540074

Quality assurance (QA) for environmental analysis is a growing feature of the nineties as is illustrated by the number of QA guidelines and systems which are being implemented nowadays. There is, however, often a huge gap between the implementation and respect of QA guidelines and the technical approach undertaken to improve and validate new analytical methods. This is particularly true for complex determinations involving multi-step methodologies such as those used in speciation and organic analyses.Quality assurance may also be considered from the technical point of view, which is the focus of this book. The techniques used in different analytical fields (inorganic, speciation and organic analysis) are critically reviewed (i.e. discussion of advantages and limitations) and existing tools for evaluating their performance are described (e.g. interlaboratory studies, use of certified reference materials). Particular reference is made to the activities of the Measurements and Testing Programme (BCR) of the European Commission towards the improvement of quality control of environmental analysis.The book has been written by experienced practitioners. By its nature, it serves as a practical reference for postgraduate students and environmental chemists who need a wide overview of the techniques used in environmental analysis and existing ways of evaluating the performance of relevant analytical methods. The critical discussions of the methods described, as well as the development of quality assurance aspects, makes it unique.

Chromatographic Analysis of the Environment

Chromatographic Analysis of the Environment
Author: Leo M.L. Nollet
Publisher: CRC Press
Total Pages: 650
Release: 2017-03-03
Genre: Technology & Engineering
ISBN: 1315316196

This detailed handbook covers different chromatographic analysis techniques and chromatographic data for compounds found in air, water, and soil, and sludge. The new edition outlines developments relevant to environmental analysis, especially when using chromatographic mass spectrometric techniques. It addresses new issues, new lines of discussion, and new findings, and develops in greater detail the aspects related to chromatographic analysis in the environment. It also includes different analytical methodologies, addresses instrumental aspects, and outlines conclusions and perspectives for the future.

Methods for Environmental Trace Analysis

Methods for Environmental Trace Analysis
Author: John R. Dean
Publisher: John Wiley & Sons
Total Pages: 284
Release: 2003-07-11
Genre: Science
ISBN: 0470861320

Provides the basic skills and information required to prepare an environmental sample for analysis. Divided into two sections, i.e. Inorganic Analysis and Organic Analysis, this book covers selected techniques, principally atomic spectroscopy and chromatography. Using flow diagrams to augment the experimental information, it highlights the most appropriate methods and the likely results. Detailed experimental information provided in an easy-to-follow style with illustrations Describes the specific sample preparation approaches necessary to analyse a particular sample type Discussion of selected literature sources highlights the most appropriate methods and the likely results obtained

A Practical Guide to Graphite Furnace Atomic Absorption Spectrometry

A Practical Guide to Graphite Furnace Atomic Absorption Spectrometry
Author: David J. Butcher
Publisher: John Wiley & Sons
Total Pages: 282
Release: 1998-03-23
Genre: Science
ISBN: 9780471125532

Die Atomabsorptionsspektroskopie mit Graphitrohrküvetten wird vor allem in der Material- und Umweltwissenschaft zur Untersuchung von Legierungen, Keramiken, Polymeren, Kompositwerkstoffen und Abwässern eingesetzt. Dieses umfangreiche Handbuch enthält viele praktische Beispiele, Tips und Tricks sowie Angaben zur instrumentellen Ausrüstung, zu modernen Entwicklungen und zur Fehlersuche: Eine wahre Fundgrube für den Praktiker, jedoch auch für Einsteiger geeignet - mit verschiedenen Anhängen, historischen Hintergrundinformationen, Literaturverzeichnissen und einem Glossar der verwendeten Fachterminologie. (06/98)

Trace Element Speciation for Environment, Food and Health

Trace Element Speciation for Environment, Food and Health
Author: L Ebdon
Publisher: Royal Society of Chemistry
Total Pages: 419
Release: 2007-10-31
Genre: Technology & Engineering
ISBN: 184755220X

The ongoing progress of science has shown that it is important for analytical scientists to determine not only the presence of particular elements, but also their species. There are many fields where this is applicable, and where there are a number of topics to be addressed. Developing separation and measurement systems for the many element species has tested the resourcefulness of analytical chemists over recent decades. A product of the EU sponsored Speciation 21 Network, this book presents a detailed review of the state-of-the-art of speciation issues in the occupational health, food and environment sectors, along with the main conclusions arising from discussions held during expert meetings. Topics covered include mercury and organotin compounds in the environment; factors affecting the health of workers; the importance of speciation of trace elements for health, and subsequent metabolism in the body; analytical methodologies; risk assessment; and legislation. Trace Element Speciation for Environment, Food and Health provides an insight into applied research in the speciation field and how it has become so important in all the fields represented. With its comprehensive coverage, it will be of particular interest to researchers in industry and academia, as well as government agencies and legislative bodies.

Flow Analysis with Atomic Spectrometric Detectors

Flow Analysis with Atomic Spectrometric Detectors
Author: A. Sanz-Medel
Publisher: Elsevier
Total Pages: 489
Release: 1999-02-25
Genre: Science
ISBN: 0080531709

Flow Analysis (FA) offers a very convenient and fast approach to enhance and automate 'preliminary steps' of analysis (sample dissolution, pretreatments, preconcentrations, etc.) for atomic spectrometric detectors (ASD). Moreover, flow manifolds can ease the well-known problem of sample introduction/presentation to atomisers or even expand the classical scope of atomic/elemental information, characterizing atomic spectrometry, into the realm of molecules and metal-compounds analysis (e.g. by resorting to coupled separation techniques). All these facts could explain both the extraordinary interest for research and the great importance for practical problem-solving achieved nowadays by FA-ASD.On the threshold of the new millennium when plasma emission and mass spectrometry are so important and popular, the editor considered it timely to produce a book which covers all present atomic detectors and techniques where FA has been or can be advantageously employed. The book has been conceived in three separate parts:Part I gives the fundamental, instrumentation and potential of FIA as a most versatile sample presentation/introduction system for atomic spectrometry.Part II provides a modern account of fundamentals, possibilities and applications offered by flow analysis to atomic spectrometry for on-line sample pretreatments, separations and preconcentrations.Part III deals with applications of FA-ASD combinations to analytical problem-solving in most varied fields and situations.This monograph integrates the most popular aspects of FIA, its new developments for sample on-line treatments and on-line non-chromatographic and chromatographic separations (all typical 'flow analysis') in connection with all branches of analytical atomic spectrometry. Thus, academics, researchers and routine users of analytical atomic spectrometry will find this book invaluable.

Trace Analysis

Trace Analysis
Author: Peter Bedson
Publisher: Royal Society of Chemistry
Total Pages: 420
Release: 2007-10-31
Genre: Science
ISBN: 1847559409

Trace Analysis is a highly practical book which deals with the science rather than the paperwork of quality assurance systems. Produced as part of the UK Valid Analytical Measurement (VAM) initiative, it provides the analyst with a systematic approach across the broad spectrum of trace analysis, offering practical advice and guidance on methodology and techniques. The book is structured to take the analyst step-by-step through the stages of any trace analysis. The approach is general, being broken down only into types of analyte. Additional chapters explain the application of groups of techniques to each analyte type. Each section contains references to published material which will allow the analyst to obtain further information on specific topics. Throughout the book, the analyst is reminded of pitfalls which lead to unreliable results. This new book therefore offers invaluable advice to analysts in all areas and at all levels, providing practical 'expert' advice on methodology. It will prove indispensable as a single, comprehensive bench guide for analysts in university, college and industrial laboratories.

Atomic Absorption Spectrometry in Occupational and Environmental Health Practice

Atomic Absorption Spectrometry in Occupational and Environmental Health Practice
Author: Dimiter L. Tsalev
Publisher: CRC Press
Total Pages: 374
Release: 1995-05-17
Genre: Science
ISBN: 9780849349997

This new, self-contained volume covers in a critical, exhaustive, and in-depth manner the progress in AAS determinations of 55 chemical elements in 42 individual chapters, with an emphasis on the latest instrumental and methodological developments. These include Zeeman background correction, the Stabilized Temperature Platform Atomizer (STPA), flow-injection and continuous-flow approaches, slurry and solid sampling, efficient chemical modification, on-line sample pretreatment/enrichment, speciation, availability of QC materials, alternative analytical techniques, and more. A key to this vast application area is provided by well-organized tabulated information, including outlines of 782 selected AAS procedures for analysis of blood, serum, urine, hair, nail, teeth, tissues, food, and other relevant biological specimens. More than 2100 AAS papers are included in a unique bibliography of 3223 up-to-date references spanning the last 13 years.