Chemistry Experiments for Instrumental Methods

Chemistry Experiments for Instrumental Methods
Author: Donald T. Sawyer
Publisher: John Wiley & Sons
Total Pages: 454
Release: 1984-09-03
Genre: Science
ISBN:

Potentiometric methods; Conductometric methods; Controlled potential methods (voltammetry); Electrolytic methods and controlled-current methods; Analytical ultraviolet-visible absorption spectroscopy; Absorption spectroscopy of electronic transitions; Infrared spectroscopy; Atomic absorption and atomic emission spectroscopy; Fluorescence spectroscopy; Nuclear magnetic resonance spectroscopy; Gas chromatography; High performance liquid chromatography (HPLC); Exclusion chromatography; Ion-exchange chromatography; Liquid-solid chromatography; Thin-layer chromatography (TCL); Electrophoresis.

Instrumental Methods in Electrochemistry

Instrumental Methods in Electrochemistry
Author: D Pletcher
Publisher: Elsevier
Total Pages: 444
Release: 2001-04-01
Genre: Science
ISBN: 1782420541

Using 372 references and 211 illustrations, this book underlines the fundamentals of electrochemistry essential to the understanding of laboratory experiments. It treats not only the fundamental concepts of electrode reactions, but also covers the methodology and practical application of the many versatile electrochemical techniques available. - Underlines the fundamentals of electrochemistry essential to the understanding of laboratory experiments - Treats the fundamental concepts of electrode reactions - Covers the methodology and practical application of the many versatile electrochemical techniques available

Environmental Laboratory Exercises for Instrumental Analysis and Environmental Chemistry

Environmental Laboratory Exercises for Instrumental Analysis and Environmental Chemistry
Author: Frank M. Dunnivant
Publisher: John Wiley & Sons
Total Pages: 416
Release: 2004-11-26
Genre: Science
ISBN: 0471660272

A comprehensive set of real-world environmental laboratoryexperiments This complete summary of laboratory work presents a richlydetailed set of classroom-tested experiments along with backgroundinformation, safety and hazard notes, a list of chemicals andsolutions needed, data collection sheets, and blank pages forcompiling results and findings. This useful resource also: Focuses on environmental, i.e., "dirty" samples Stresses critical concepts like analysis techniques anddocumentation Includes water, air, and sediment experiments Includes an interactive software package for pollutant fate andtransport modeling exercises Functions as a student portfolio of documentationabilities Offers instructors actual samples of student work fortroubleshooting, notes on each procedure, and procedures forsolutions preparation.

Instrumental Analytical Chemistry

Instrumental Analytical Chemistry
Author: James W. Robinson
Publisher: CRC Press
Total Pages: 920
Release: 2021-06-29
Genre: Science
ISBN: 1315301148

Analytical chemistry today is almost entirely instrumental analytical chemistry and it is performed by many scientists and engineers who are not chemists. Analytical instrumentation is crucial to research in molecular biology, medicine, geology, food science, materials science, and many other fields. With the growing sophistication of laboratory equipment, there is a danger that analytical instruments can be regarded as "black boxes" by those using them. The well-known phrase "garbage in, garbage out" holds true for analytical instrumentation as well as computers. This book serves to provide users of analytical instrumentation with an understanding of their instruments. This book is written to teach undergraduate students and those working in chemical fields outside analytical chemistry how contemporary analytical instrumentation works, as well as its uses and limitations. Mathematics is kept to a minimum. No background in calculus, physics, or physical chemistry is required. The major fields of modern instrumentation are covered, including applications of each type of instrumental technique. Each chapter includes: A discussion of the fundamental principles underlying each technique Detailed descriptions of the instrumentation. An extensive and up to date bibliography End of chapter problems Suggested experiments appropriate to the technique where relevant This text uniquely combines instrumental analysis with organic spectral interpretation (IR, NMR, and MS). It provides detailed coverage of sampling, sample handling, sample storage, and sample preparation. In addition, the authors have included many instrument manufacturers’ websites, which contain extensive resources.

Practical Instrumental Analysis

Practical Instrumental Analysis
Author: Sergio Petrozzi
Publisher: John Wiley & Sons
Total Pages: 388
Release: 2012-09-24
Genre: Science
ISBN: 3527665919

This practical book in instrumental analytics conveys an overview of important methods of analysis and enables the reader to realistically learn the (principally technology-independent) working techniques the analytical chemist uses to develop methods and conduct validation. What is to be conveyed to the student is the fact that analysts in their capacity as problem-solvers perform services for certain groups of customers, i.e., the solution to the problem should in any case be processed in such a way as to be "fit for purpose". The book presents sixteen experiments in analytical chemistry laboratory courses. They consist of the classical curriculum used at universities and universities of applied sciences with chromatographic procedures, atom spectrometric methods, sensors and special methods (e.g. field flow fractionation, flow injection analysis and N-determination according to Kjeldahl). The carefully chosen combination of theoretical description of the methods of analysis and the detailed instructions given are what characterizes this book. The instructions to the experiments are so detailed that the measurements can, for the most part, be taken without the help of additional literature. The book is complemented with tips for effective literature and database research on the topics of organization and the practical workflow of experiments in analytical laboratory, on the topic of the use of laboratory logs as well as on writing technical reports and grading them (Evaluation Guidelines for Laboratory Experiments). A small introduction to Quality Management, a brief glance at the history of analytical chemistry as well as a detailed appendix on the topic of safety in analytical laboratories and a short introduction to the new system of grading and marking chemicals using the "Globally Harmonized System of Classification and Labelling of Chemicals (GHS)", round off this book. This book is therefore an indispensable workbook for students, internship assistants and lecturers (in the area of chemistry, biotechnology, food technology and environmental technology) in the basic training program of analytics at universities and universities of applied sciences.

Chemical Analysis

Chemical Analysis
Author: Francis Rouessac
Publisher: John Wiley & Sons
Total Pages: 494
Release: 2013-05-06
Genre: Science
ISBN: 1118681878

Completely revised and updated, Chemical Analysis: Second Edition is an essential introduction to a wide range of analytical techniques and instruments. Assuming little in the way of prior knowledge, this text carefully guides the reader through the more widely used and important techniques, whilst avoiding excessive technical detail. Provides a thorough introduction to a wide range of the most important and widely used instrumental techniques Maintains a careful balance between depth and breadth of coverage Includes examples, problems and their solutions Includes coverage of latest developments including supercritical fluid chromatography and capillary electrophoresis

Instrumental Methods in Metal Ion Speciation

Instrumental Methods in Metal Ion Speciation
Author: Imran Ali
Publisher: CRC Press
Total Pages: 376
Release: 2006-03-14
Genre: Medical
ISBN: 1420019406

The knowledge of metal ion speciation is essential for predicting the exact toxicities of metal ion species in the environment. Metal ions can exist in various oxidation states, each of which possesses different physical and chemical properties as well as exhibit varying toxicities. Often, toxicity data is unreliable because it is based on metal io

Practical Inorganic Chemistry

Practical Inorganic Chemistry
Author: G. Pass
Publisher: Springer Science & Business Media
Total Pages: 254
Release: 2013-03-09
Genre: Science
ISBN: 9401727449

In revising the text opportunity has been taken to introduce SI units throughout. An Appendix has been included which contains tables of SI units and a table of conversion factors for use when consulting data in non-SI units. Chapter 19 now includes experiments demon strating the use of ion-exchange and solid-liquid chromatography_ Exercises involving colorimetry have been included in Chapter 17. These techniques are introduced as part of a complementary exercise where their relevance is seen as part of a complete piece of work. Minor improvements have been made to some of the experimental procedures and we are grateful to those who have made helpful suggestions in this respect. G. PASS H. SUTCLIFFE iii Preface to the First Edition The student of inorganic chemistry is fortunate in having a wide choice of textbooks covering the descriptive and theoretical aspects of the sUbject. There is no comparable choice of textbooks covering practical inorganic chemistry. Moreover, there is a tendency for many students to draw an unfortunate distinction between chemistry taught in the lecture room, and laboratory work. Consideration of these points prompted the preparation of this book, in which we have attempted to emphasize the relationship between theory and practice.

A Practical Guide to Instrumental Analysis

A Practical Guide to Instrumental Analysis
Author: Erno Pungor
Publisher: CRC Press
Total Pages: 404
Release: 2020-11-25
Genre: Science
ISBN: 1000142442

A Practical Guide to Instrumental Analysis covers basic methods of instrumental analysis, including electroanalytical techniques, optical techniques, atomic spectroscopy, X-ray diffraction, thermoanalytical techniques, separation techniques, and flow analytical techniques. Each chapter provides a brief theoretical introduction followed by basic and special application experiments. This book is ideal for readers who need a knowledge of special techniques in order to use instrumental methods to conduct their own analytical tasks.

Laboratory Experiments in Analytical Chemistry

Laboratory Experiments in Analytical Chemistry
Author: Maurice O. Iwunze
Publisher:
Total Pages: 280
Release: 2005-08
Genre: Science
ISBN: 9781420850703

In the recent past quantitative chemical analysis textbook writers included selected experiments to complete and complement the text and thus give instructors a choice to select the experiments to be performed by students in quantitative analysis course. On the other hand, this is not so for courses in instrumental analysis which is a sequential course to quantitative analysis. This is, perhaps, due to the numerous instrumental techniques that have been developed over the years for chemical analysis. In its stead, textbooks on experiments in instrumental analysis are common, and these are as diversified as the topics covered in lecture courses. Most of the experimental topics covered, especially, in quantitative analysis, lean heavily on determination of materials or compounds of inorganic chemistry origin. This seems to be the tradition with only a few exceptions. However, recently, textbooks on quantitative analysis have emerged and continue to emerge, without any experimental section. This is not quite surprising though, since many instructors nowadays, tend to design their own experiments to suit and complement their lecture materials. On the other hand, the trend in the production of books on instrumental analysis experiments has remained the same. The objective of this book is therefore two fold. One is to design a reasonably comprehensive laboratory text that embodies both areas of analytical chemistry. The other is to shy away from the tradition of making quantitative analysis experiments lean too heavily on inorganic materials. To this end, several topics ranging from inorganic to organic materials are included in this laboratory text book. A new element is also introduced in this book. That is, students are exposed throughout the book to the analysis of compounds of pharmaceutical relevance.