Chemically Modified Electrodes
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| Author | : Jacques Simonet |
| Publisher | : World Scientific |
| Total Pages | : 449 |
| Release | : 2017-10-13 |
| Genre | : Science |
| ISBN | : 1786342456 |
This book documents Professor Jacques Simonet's contribution to building new electrode materials and their related catalytic reactions. Research includes synthesis of new alloys of palladium, discovery of new composite electrodes (including gold- and silver-graphene) and the creation of new materials through judicious cathodic or anodic doping. Additionally, studies demonstrate the malleability and reactivity of previously unused precious and semi-precious metals for the creation of 2D and 3D catalytic materials. Studies key to innovative research show how transition metals may reversibly cathodically insert small size electro-active molecules such as CO2 and O2, and be applied to methods of depollution brought by carbon and nitrogen oxides.Written for practical use, Simonet has provided both theory and tools needed for those aiming to recreate and develop his experiments in electrochemical catalysis and surface modifications. This full publication of research gives graduate and post-graduate students of chemistry, electrochemistry and catalysis an in-depth insight into key historical and modern developments in the field.
| Author | : |
| Publisher | : John Wiley & Sons |
| Total Pages | : 278 |
| Release | : 2009-07-10 |
| Genre | : Science |
| ISBN | : 9783527627066 |
With contributions from an international group of expert authors, this book includes the latest trends in tailoring interfacial properties electrochemically. The chapters cover various organic and inorganic compounds, with applications ranging from electrochemistry to nanotechnology and biology. Of interest to physical, surface and electrochemists, materials scientists and physicists.
| Author | : Cynthia G. Zoski |
| Publisher | : Elsevier |
| Total Pages | : 935 |
| Release | : 2007-02-07 |
| Genre | : Science |
| ISBN | : 0444519580 |
Electrochemistry plays a key role in a broad range of research and applied areas including the exploration of new inorganic and organic compounds, biochemical and biological systems, corrosion, energy applications involving fuel cells and solar cells, and nanoscale investigations. The Handbook of Electrochemistry serves as a source of electrochemical information, providing details of experimental considerations, representative calculations, and illustrations of the possibilities available in electrochemical experimentation. The book is divided into five parts: Fundamentals, Laboratory Practical, Techniques, Applications, and Data. The first section covers the fundamentals of electrochemistry which are essential for everyone working in the field, presenting an overview of electrochemical conventions, terminology, fundamental equations, and electrochemical cells, experiments, literature, textbooks, and specialized books. Part 2 focuses on the different laboratory aspects of electrochemistry which is followed by a review of the various electrochemical techniques ranging from classical experiments to scanning electrochemical microscopy, electrogenerated chemiluminesence and spectroelectrochemistry. Applications of electrochemistry include electrode kinetic determinations, unique aspects of metal deposition, and electrochemistry in small places and at novel interfaces and these are detailed in Part 4. The remaining three chapters provide useful electrochemical data and information involving electrode potentials, diffusion coefficients, and methods used in measuring liquid junction potentials. * serves as a source of electrochemical information * includes useful electrochemical data and information involving electrode potentials, diffusion coefficients, and methods used in measuring liquid junction potentials * reviews electrochemical techniques (incl. scanning electrochemical microscopy, electrogenerated chemiluminesence and spectroelectrochemistry)
| Author | : R. Kossowsky |
| Publisher | : Springer Science & Business Media |
| Total Pages | : 766 |
| Release | : 2012-12-06 |
| Genre | : Technology & Engineering |
| ISBN | : 9400962169 |
Over the last few years there has been increasing need for systematic and straregically designed experiments of surface morphology evolution resulting form ion bombardment induced sputtering. Although there is an impressive number of investi gations {1} concerned with semiconductor materials as a result of immediate applications, the most systematic investigations have been conducted with fcc metals with particular interest on single crystal Cu {2,3}. Evidence now exists that within certain para meters (i. e ion species (Ar+), ion energy (20-44 KeV), substrate 2 temperature (80-550° K), dose rate (100-500 gA cm- ) , residual x 5 9 pressure (5 10- to 5x10- mm Hg) and polar and azimuthal angle of ion incidence {4} reproducible surface morphology (etch pits and pyramids) is achieved on the (11 3 1) specific crystallographic orientation. The temporal development of individual surface features was alsoobserved in this laterstudy {4}, by employing an in situ ion source in the scanning electron microscope at Salford, a technique also empolyed in studies of the influence of polar angle of ion incidence {5} and surface contaminants {6} on the topographyof Ar+ bombarded Si. Studies have also been made on the variation of incident ion species with the (11 3 1) Cu surface and it was fully recognized {7} that residual surface contaminants when present could playa major role in dictating the morhological evolution.
| Author | : Sami Elhag |
| Publisher | : Linköping University Electronic Press |
| Total Pages | : 89 |
| Release | : 2017-02-02 |
| Genre | : |
| ISBN | : 9176855902 |
The goal of this thesis is the development of scalable, low cost synthesis of metal oxide nanostructures based electrodes and to correlate the chemical modifications with their energy conversion performance. Methods in energy conversion in this thesis have focused on two aspects; a potentiometric chemical sensor was used to determine the analytical concentration of some components of the analyte solution such as dopamine, glucose and glutamate molecules. The second aspect is to fabricate a photo-electrochemical (PEC) cell. The biocompatibility, excellent electro-catalytic activities and fast electron transfer kinetics accompanied with a high surface area to volume ratio; are properties of some metal oxide nanostructures that of a potential for their use in energy conversion. Furthermore, metal oxide nanostructures based electrode can effectively be improved by the physical or a chemical modification of electrode surface. Among these metal oxide nanostructures are cobalt oxide (Co3O4), zinc oxide (ZnO), and bismuth-zincvanadate (BiZn2VO6) have all been studied in this thesis. Metal oxide nanostructures based electrodes are fabricated on gold-coated glass substrate by low temperature (< 100 0C) wet chemicalapproach. X-ray diffraction, x-ray photoelectron spectroscopy and scanning electron microscopy were used to characterize the electrodes while ultraviolet-visible absorption and photoluminescence were used to investigate the optical properties of the nanostructures. The resultant modified electrodes were tested for their performance as chemical sensors and for their efficiency in PEC activities. Efficient chemically modified electrodes were demonstrated through doping with organic additives like anionic, nonionic or cationic surfactants. The organic additives are showing a crucial role in the growth process of metal oxide nanocrystals and hence can beused to control the morphology. These organic additives act also as impurities that would significantly change the conductivity of the electrodes. However, no organic compounds dependence was observed to modify the crystallographic structure. The findings in this thesis indicate the importance of the use of controlled nanostructures morphology for developing efficient functional materials.
| Author | : M. Anderson |
| Publisher | : The Electrochemical Society |
| Total Pages | : 45 |
| Release | : 2015-04-30 |
| Genre | : Science |
| ISBN | : 1607686155 |
| Author | : Joseph Wang |
| Publisher | : John Wiley & Sons |
| Total Pages | : 228 |
| Release | : 2004-03-24 |
| Genre | : Science |
| ISBN | : 0471460796 |
The critically acclaimed guide to the principles, techniques, and instruments of electroanalytical chemistry-now expanded and revised Joseph Wang, internationally renowned authority on electroanalytical techniques, thoroughly revises his acclaimed book to reflect the rapid growth the field has experienced in recent years. He substantially expands the theoretical discussion while providing comprehensive coverage of the latest advances through late 1999, introducing such exciting new topics as self-assembled monolayers, DNA biosensors, lab-on-a-chip, detection for capillary electrophoresis, single molecule detection, and sol-gel surface modification. Along with numerous references from the current literature and new worked-out examples, Analytical Electrochemistry, Second Edition offers clear, reader-friendly explanations of the fundamental principles of electrochemical processes as well as important insight into the potential of electroanalysis for problem solving in a wide range of fields, from clinical diagnostics to environmental science. Key topics include: The basics of electrode reactions and the structure of the interfacial region Tools for elucidating electrode reactions and high-resolution surface characterization An overview of finite-current controlled potential techniques Electrochemical instrumentation and electrode materials Principles of potentiometric measurements and ion-selective electrodes Chemical sensors, including biosensors, gas sensors, solid-state devices, and sensor arrays
| Author | : Peter Kissinger |
| Publisher | : CRC Press |
| Total Pages | : 1014 |
| Release | : 1996-01-23 |
| Genre | : Science |
| ISBN | : 9780824794453 |
This volume provides a practical, intuitive approach to electroanalytical chemistry, presenting fundamental concepts and experimental techniques without the use of technical jargon or unnecessarily extensive mathematics. This edition offers new material on ways of preparing and using microelectrodes, the processes that govern the voltammetric behavior of microelectrodes, methods for characterizing chemically modified electrodes, electrochemical studies at reduced temperatures, and more. The authors cover such topics as analog instrumentation, overcoming solution resistance with stability and grace in potentiostatic circuits, conductivity and conductometry, electrochemical cells, carbon electrodes, film electrodes, microelectrodes, chemically modified electrodes, mercury electrodes, and solvents and supporting electrolytes.
| Author | : Ewa Schab-Balcerzak |
| Publisher | : BoD – Books on Demand |
| Total Pages | : 230 |
| Release | : 2011-12-22 |
| Genre | : Science |
| ISBN | : 9533076933 |
In recent years, great focus has been placed upon polymer thin films. These polymer thin films are important in many technological applications, ranging from coatings and adhesives to organic electronic devices, including sensors and detectors. Electrochemical polymerization is preferable, especially if the polymeric product is intended for use as polymer thin films, because electrogeneration allows fine control over the film thickness, an important parameter for fabrication of devices. Moreover, it was demonstrated that it is possible to modify the material properties by parameter control of the electrodeposition process. Electrochemistry is an excellent tool, not only for synthesis, but also for characterization and application of various types of materials. This book provides a timely overview of a current state of knowledge regarding the use of electropolymerization for new materials preparation, including conducting polymers and various possibilities of applications.
| Author | : Skotheim |
| Publisher | : CRC Press |
| Total Pages | : 288 |
| Release | : 1988-05-27 |
| Genre | : Science |
| ISBN | : 9780824779689 |
Keeping pace with this rapidly expanding and dynamic field, this important reference presents detailed topical reviews of new advances in electroresponsive molecular and polymeric research -- stimulating productive interaction and exchange of ideas between disciplines. Written by leading authorities in industry and academia, Electroresponsive Molecular and Polymeric Systems incorporates theory, synthesis, and technological applications. This informative, up-to-date resource discusses the synthesis of new electronically conducting polymers ... considers recent theoretical developments in conductivity mechanisms ... reviews the status of piezo- and pyroelectric polymers, particularly their performance in commercial devices ... analyzes the structure and transport properties of ion-conducting polymers ... and explores structures and properties of redox polymeric systems. Illustrated with useful diagrams, equations, and drawings, and containing over 800 references, the volume is indispensable reading for all polymer scientists and engineers; solid state physicists; physical, surface, and electro- chemists; and upper-level undergraduate and graduate students in the above disciplines. Book jacket.
