Capillary Gas Chromatography
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| Author | : Walter Jennings |
| Publisher | : Elsevier |
| Total Pages | : 335 |
| Release | : 2012-12-02 |
| Genre | : Science |
| ISBN | : 0323138217 |
The need for this second edition is dictated by developments that have occurred in this rapidly changing field and by sins of omission and sins of commission in the first edition. Projections available at the time of this writing indicate that gas chromoatography will remain the world's most widely used analytical technique for some time.
| Author | : Dean Rood |
| Publisher | : Wiley-VCH |
| Total Pages | : 352 |
| Release | : 1999-03-02 |
| Genre | : Science |
| ISBN | : |
Dean Rood A Practical Guide to the Care, Maintenance, and Troubleshooting of Capillary Gas Chromatographic Systems Third, Revised Edition The field of gas chromatography continues the evolutionary process. This is well demonstrated by the continuous series of developments — in columns, equipment, apparatus, techniques, and applications — that have occured since the publication of the first edition of this very successful offering. Problems experienced by users differ from case to case, and these differences sometimes necessitate different approaches to care, maintenance, and trouble-shooting. This book is intended for the average GC user and not for those whose entire life revolves around capillary gas chromatography. The topics covered within these pages are based on the most common problems, questions, and misconceptions about capillary gas chromatography. These topics have been assembled and presented in a unique, practical, and concise format suitable even for the most inexperienced user. The author has not changed his successful approach to the topic in the present third edition. Instead, he has focused on updating and correcting the text of the widely acclaimed second edition.
| Author | : Walter Jennings |
| Publisher | : Academic Press |
| Total Pages | : 486 |
| Release | : 1980-10-28 |
| Genre | : Science |
| ISBN | : |
Qualitative Analysis of Flavor and Fragrance Volatiles by Glass Capillary Gas Chromatography deals with the application of glass capillary gas chromatography to qualitative analysis of flavor and fragrance volatiles. Topics range from gas chromatographic system requirements and retention indices to selective detectors, ancillary reactions, and gas chromatography-mass spectrometry. This text is comprised of six chapters; the first of which provides an overview of the use of glass capillary gas chromatography in qualitative analysis of flavor and fragrance volatiles. The discussion then turns to gas chromatographic system requirements with respect to columns, inlets, detectors, and temperature control. The reader is also introduced to the Kovats retention index system, which utilizes a logarithmic scale to describe the retention behavior of a compound relative to that of the n-paraffin hydrocarbons. The use of selective detectors, such as thermal conductivity, flame ionization, nitrogen-phosphorus, electron capture, and photoionization detectors in qualitative analysis, is also considered. The final two chapters focus on ancillary reactions in glass capillary gas chromatography and general considerations in gas chromatography-mass spectrometry, including interfacing. This book is intended primarily for researchers involved in studies of the volatile constituents of fragrances, food, and natural products.
| Author | : Pat Sandra |
| Publisher | : |
| Total Pages | : 464 |
| Release | : 1987 |
| Genre | : Chromatographic analysis |
| ISBN | : |
Introduction to essential oil analysis. some aspects of essential oil preparation. considerations on the selection of cappilary columns for essential oil analysis. microtechniques in essential oil analysis. headscape versus classical analysis. Fingerprints in essential oil analysis. industrial quality control of essential oil by capillary GC. Retention indices in essential oil analysis. Possibilities and results of dual channel analysis of essential oils with fused silica capillaru columns. GC- mass specytrometry of essential oils: positive ion and negative ion and negative ion chemical ionazation techniques,computer matching techniques. Examples of artefact formation by chromatographic techniques. Possibilities, limitations, and future develpments in GC-FTIR analysis of essential oils. Possibilities of multidimensional GC in essential oils.
| Author | : Dean Rood |
| Publisher | : John Wiley & Sons |
| Total Pages | : 344 |
| Release | : 2007-09-24 |
| Genre | : Science |
| ISBN | : 3527611312 |
This fourth edition of the classic guide for every user of gas chromatographic instrumentation is now updated to include such new topics as fast GC using narrow, short columns, electronic pressure control, and basic aspects of quantitative gas chromatography. The author shares his many years of experience in technical support for gas chromatography users, addressing the most common problems, questions and misconceptions in capillary gas chromatography. He structures and presents the material in a concise and practical manner, suitable even for the most inexperienced user without any detailed knowledge of chemistry or chromatography. For lab technicians in chemistry, analytical, food, medicinal and environmental chemists, pharmaceutists.
| Author | : Robert L. Grob, PhD |
| Publisher | : John Wiley & Sons |
| Total Pages | : 1059 |
| Release | : 2004-08-04 |
| Genre | : Science |
| ISBN | : 047165115X |
The bible of gas chromatography-offering everything the professional and the novice need to know about running, maintaining, and interpreting the results from GC Analytical chemists, technicians, and scientists in allied disciplines have come to regard Modern Practice of Gas Chomatography as the standard reference in gas chromatography. In addition to serving as an invaluable reference for the experienced practitioner, this bestselling work provides the beginner with a solid understanding of gas chromatographic theory and basic techniques. This new Fourth Edition incorporates the most recent developments in the field, including entirely new chapters on gas chromatography/mass spectrometry (GC/MS); optimization of separations and computer assistance; high speed or fast gas chromatography; mobile phase requirements: gas system requirements and sample preparation techniques; qualitative and quantitative analysis by GC; updated information on detectors; validation and QA/QC of chromatographic methods; and useful hints for good gas chromatography. As in previous editions, contributing authors have been chosen for their expertise and active participation in their respective areas. Modern Practice of Gas Chromatography, Fourth Edition presents a well-rounded and comprehensive overview of the current state of this important technology, providing a practical reference that will greatly appeal to both experienced chomatographers and novices.
| Author | : Karl-Heinz Kubeczka |
| Publisher | : Wiley |
| Total Pages | : 0 |
| Release | : 2002-05-22 |
| Genre | : Science |
| ISBN | : 9780471963141 |
In addition to capillary gas chromatography and GC-MS, carbon-13 NMR spectroscopy provides an alternative method for essential oils analysis. The excellent visual spacing of the signals enables oil samples to be analyzed without preliminary separation of their components. Also, information relating to the molecular structure of the oil constituents can be ascertained from the measured chemical shifts. This second edition clearly demonstrates the power of the technique in the characterization of essential oils, based on 60 sample oils chosen for their industrial importance together with the 188 carbon-13 NMR spectra of significant components. Supporting data are presented using capillary gas chromatography. Key features of the Second Edition: * 18 new essential oils are included, five oils are replaced and five oils with less or little importance are deleted * Revision of numerous analyses taken over from the 1st edition * Capillary gas chromatograms of 60 commercially important essential oils * Qualitative and quantitative analytical results of those essential oils * Carbon-13 NMR analyses of those essential oils without separation of their components * Carbon-13 NMR spectra of 188 most important oil constituents are given (67 are new in the 2nd edition) This collection of 13C NMR and GC data is aimed at essential oils and natural products chemists, NMR research groups, university departments of chemistry, pharmacy, botany, and food science, as well as those working in the essential oils, perfumes, flavours and food technology industries.
| Author | : Harold M. McNair |
| Publisher | : John Wiley & Sons |
| Total Pages | : 195 |
| Release | : 2011-09-20 |
| Genre | : Science |
| ISBN | : 1118211200 |
The New Edition of the Well-Regarded Handbook on Gas Chromatography Since the publication of the highly successful first edition of Basic Gas Chromatography, the practice of chromatography has undergone several notable developments. Basic Gas Chromatography, Second Edition covers the latest in the field, giving readers the most up-to-date guide available, while maintaining the first edition's practical, applied approach to the subject and its accessibility to a wide range of readers. The text provides comprehensive coverage of basic topics in the field, such as stationary phases, packed columns and inlets, capillary columns and inlets, detectors, and qualitative and quantitative analysis. At the same time, the coverage also features key additions and updated topics including: Gas chromatography-mass spectrometry (GC-MS) Sampling methods Multidimensional gas chromatography Fast gas chromatography Gas chromatography analysis of nonvolatile compounds Inverse gas chromatography and pyrolysis gas chromatography Along with these new and updated topics, the references, resources, and Web sites in Basic Gas Chromatography have been revised to reflect the state of the field. Concise and fundamental in its coverage, Basic Gas Chromatography, Second Edition remains the standard handbook for everyone from undergraduates studying analytical chemistry to working industrial chemists.
| Author | : Eugene F. Barry |
| Publisher | : John Wiley & Sons |
| Total Pages | : 315 |
| Release | : 2007-04-27 |
| Genre | : Science |
| ISBN | : 0470114177 |
Choosing the right column is key in Gas Chromatography Gas Chromatography (GC) is the most widely used method for separating and analyzing a wide variety of organic compounds and gases. There have been many recent advancements in both packed column and capillary column GC. With numerous options and considerations, selecting the right column can be complicated. This resource provides essential guidance for scientists and technicians, including: Methods of choosing both capillary and packed columns Selection of dimensions (column length, I.D., film thickness, etc.) and type of column Guidelines for proper connections of the column to the injector and detector United States Pharmacopeia and National Formulary chromatographic methods ASTM, EPA, NIOSH, and OSHA column selection specifications Information on the advantages of computer assistance in GC and multidimensional GC Comprehensive information on column oven temperature control Columns for Gas Chromatography: Performance and Selection is a hands-on reference for scientists and technicians using GC.
| Author | : Konrad Grob |
| Publisher | : John Wiley & Sons |
| Total Pages | : 480 |
| Release | : 2008-11-21 |
| Genre | : Science |
| ISBN | : 3527612882 |
This comprehensive and unique handbook of split and splitless injection techniques has been completely revised and updated. This new edition offers: - New insights concerning sample evaporation in the injector - Information about matrix effects - A new chapter on injector design The real processes within the injector are for the first time visualized and explained by the CD-ROM included in the book. Furthermore the reader will understand the concepts of injection techniques and get a knowledge of the sources of error. The handbook also includes many practical guidelines. From reviews of former editions: "This substantial book is on injection techniques alone, which ... demonstrates this can have many pitfalls ... no one should be allowed to direct a laboratory doing quantitative analysis by GC without first being thoroughly familar with this book ..." The Analyst "This is a detailed reference volume filled with practical suggestions and techniques for managing split and splitless injection in the day-to-day world of the working gas chromatographer. It will be useful ... for anyone who must work hands-on with GC." Journal of High Resolution Chromatography
