Analytical Impedance Spectroscopy
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| Author | : Ramanathan Srinivasan |
| Publisher | : CRC Press |
| Total Pages | : 263 |
| Release | : 2021-05-03 |
| Genre | : Science |
| ISBN | : 1000379213 |
This book covers the fundamental aspects and the application of electrochemical impedance spectroscopy (EIS), with emphasis on a step-by-step procedure for mechanistic analysis of data. It enables the reader to learn the EIS technique, correctly acquire data from a system of interest, and effectively interpret the same. Detailed illustrations of how to validate the impedance spectra, use equivalent circuit analysis, and identify the reaction mechanism from the impedance spectra are given, supported by derivations and examples. MATLAB® programs for generating EIS data under various conditions are provided along with free online video lectures to enable easier learning. Features: Covers experimental details and nuances, data validation method, and two types of analysis – using circuit analogy and mechanistic analysis Details observations such as inductive loops and negative resistances Includes a dedicated chapter on an emerging technique (Nonlinear EIS), including code in the supplementary material illustrating simulations Discusses diffusion, constant phase element, porous electrodes, and films Contains exercise problems, MATLAB codes, PPT slide, and illustrative examples This book is aimed at senior undergraduates and advanced graduates in chemical engineering, analytical chemistry, electrochemistry, and spectroscopy.
| Author | : Vadim F. Lvovich |
| Publisher | : John Wiley & Sons |
| Total Pages | : 368 |
| Release | : 2015-11-30 |
| Genre | : Science |
| ISBN | : 1118164091 |
This book presents a balance of theoretical considerations and practical problem solving of electrochemical impedance spectroscopy. This book incorporates the results of the last two decades of research on the theories and applications of impedance spectroscopy, including more detailed reviews of the impedance methods applications in industrial colloids, biomedical sensors and devices, and supercapacitive polymeric films. The book covers all of the topics needed to help readers quickly grasp how to apply their knowledge of impedance spectroscopy methods to their own research problems. It also helps the reader identify whether impedance spectroscopy may be an appropriate method for their particular research problem. This includes understanding how to correctly make impedance measurements, interpret the results, compare results with expected previously published results form similar chemical systems, and use correct mathematical formulas to verify the accuracy of the data. Unique features of the book include theoretical considerations for dealing with modeling, equivalent circuits, and equations in the complex domain, review of impedance instrumentation, best measurement methods for particular systems and alerts to potential sources of errors, equations and circuit diagrams for the most widely used impedance models and applications, figures depicting impedance spectra of typical materials and devices, extensive references to the scientific literature for more information on particular topics and current research, and a review of related techniques and impedance spectroscopy modifications.
| Author | : Mark E. Orazem |
| Publisher | : John Wiley & Sons |
| Total Pages | : 510 |
| Release | : 2011-10-13 |
| Genre | : Science |
| ISBN | : 111820994X |
Using electrochemical impedance spectroscopy in a broad range of applications This book provides the background and training suitable for application of impedance spectroscopy to varied applications, such as corrosion, biomedical devices, semiconductors and solid-state devices, sensors, batteries, fuel cells, electrochemical capacitors, dielectric measurements, coatings, electrochromic materials, analytical chemistry, and imaging. The emphasis is on generally applicable fundamentals rather than on detailed treatment of applications. With numerous illustrative examples showing how these principles are applied to common impedance problems, Electrochemical Impedance Spectroscopy is ideal either for course study or for independent self-study, covering: Essential background, including complex variables, differential equations, statistics, electrical circuits, electrochemistry, and instrumentation Experimental techniques, including methods used to measure impedance and other transfer functions Process models, demonstrating how deterministic models of impedance response can be developed from physical and kinetic descriptions Interpretation strategies, describing methods of interpretating of impedance data, ranging from graphical methods to complex nonlinear regression Error structure, providing a conceptual understanding of stochastic, bias, and fitting errors in frequency-domain measurements An overview that provides a philosophy for electrochemical impedance spectroscopy that integrates experimental observation, model development, and error analysis This is an excellent textbook for graduate students in electrochemistry, materials science, and chemical engineering. It's also a great self-study guide and reference for scientists and engineers who work with electrochemistry, corrosion, and electrochemical technology, including those in the biomedical field, and for users and vendors of impedance-measuring instrumentation.
| Author | : Evgenij Barsoukov |
| Publisher | : John Wiley & Sons |
| Total Pages | : 498 |
| Release | : 2018-05-01 |
| Genre | : Science |
| ISBN | : 1119074088 |
The Essential Reference for the Field, Featuring Protocols, Analysis, Fundamentals, and the Latest Advances Impedance Spectroscopy: Theory, Experiment, and Applications provides a comprehensive reference for graduate students, researchers, and engineers working in electrochemistry, physical chemistry, and physics. Covering both fundamentals concepts and practical applications, this unique reference provides a level of understanding that allows immediate use of impedance spectroscopy methods. Step-by-step experiment protocols with analysis guidance lend immediate relevance to general principles, while extensive figures and equations aid in the understanding of complex concepts. Detailed discussion includes the best measurement methods and identifying sources of error, and theoretical considerations for modeling, equivalent circuits, and equations in the complex domain are provided for most subjects under investigation. Written by a team of expert contributors, this book provides a clear understanding of impedance spectroscopy in general as well as the essential skills needed to use it in specific applications. Extensively updated to reflect the field’s latest advances, this new Third Edition: Incorporates the latest research, and provides coverage of new areas in which impedance spectroscopy is gaining importance Discusses the application of impedance spectroscopy to viscoelastic rubbery materials and biological systems Explores impedance spectroscopy applications in electrochemistry, semiconductors, solid electrolytes, corrosion, solid state devices, and electrochemical power sources Examines both the theoretical and practical aspects, and discusses when impedance spectroscopy is and is not the appropriate solution to an analysis problem Researchers and engineers will find value in the immediate practicality, while students will appreciate the hands-on approach to impedance spectroscopy methods. Retaining the reputation it has gained over years as a primary reference, Impedance Spectroscopy: Theory, Experiment, and Applications once again present a comprehensive reference reflecting the current state of the field.
| Author | : Jennie Brock |
| Publisher | : |
| Total Pages | : 0 |
| Release | : 2017 |
| Genre | : Electrochemical analysis |
| ISBN | : 9781536122114 |
In Chapter One, the authors review the recent developments in the field of electrochemical impedance spectroscopy, discuss some of the challenges and compare EIS with the other relevant techniques. The effect of storage time without use (STWU) in the supporting electrolyte solution on the conducting properties of poly(o-aminophenol) (POAP) film electrodes was studied in Chapter Two. In Chapter Three, the authors study the effect of the cerium content on the corrosion behavior of Al85CexNi15-x (x = 4, 5, 6, 7 and 10) amorphous alloys obtained by melt spinning.
| Author | : Marwa El-Azazy |
| Publisher | : BoD – Books on Demand |
| Total Pages | : 169 |
| Release | : 2020-12-16 |
| Genre | : Science |
| ISBN | : 1789852153 |
Electrochemical Impedance Spectroscopy is a compendium of contributions from experts in the field of electrochemical impedance spectroscopy (EIS). This compilation of investigations and reviews addresses the groundbreaking applications of EIS in different fields. An array of exploitations are revealed throughout this book such as the use of EIS in monitoring and controlling of corrosion, in medicine where accurate information on fluid distribution is needed as well as environmental applications in food, water, and drug analyses. Competency of EIS as an approach compared to the traditional electrochemical techniques is assessed in almost every application. This book, therefore, is a valuable reference for students, researchers, and anyone interested in electrochemical impedance spectroscopy.
| Author | : Andrzej Lasia |
| Publisher | : Springer |
| Total Pages | : 376 |
| Release | : 2014-06-17 |
| Genre | : Science |
| ISBN | : 1461489334 |
This book presents a complete overview of the powerful but often misused technique of Electrochemical Impedance Spectroscopy (EIS). The book presents a systematic and complete overview of EIS. The book carefully describes EIS and its application in studies of electrocatalytic reactions and other electrochemical processes of practical interest. This book is directed towards graduate students and researchers in Electrochemistry. Concepts are illustrated through detailed graphics and numerous examples. The book also includes practice problems. Additional materials and solutions are available online.
| Author | : Lakshman Pandey |
| Publisher | : CRC Press |
| Total Pages | : 263 |
| Release | : 2023-12-22 |
| Genre | : Technology & Engineering |
| ISBN | : 1000995348 |
This book introduces the subject of impedance spectroscopy starting from fundamentals through to latest applications in areas such as ceramics, piezoelectric, sensors, agriculture, food quality control, medical diagnostics, cancer research, and so forth. Within the ambit of impedance spectroscopy, plots simulated for useful equivalent circuit models, design of sample holder, necessary precautions to be taken during measurement are described. It further discusses development of softwares for analysis of experimental data and choice of the most appropriate equivalent circuit model. All the materials are supported by problems, answers, appendices and references. Features: Includes fundamentals, equivalent circuit modeling and analysis of data related to impedance spectroscopy. Presents experimental measurements in a nuts-and-bolts approach. Includes derivation of expressions for some selected models and values of immittance functions as frequency of measurements tend to zero and to infinity. Provides clear recipe for beginners for proceeding toward developing equivalent circuit models. Describes computer program for complex nonlinear least squares fitting with example of program IMPSPEC.BAS This book is aimed at senior undergraduate/graduate students and researchers in materials engineering, mechanical engineering, electrical engineering, chemical engineering, biomedical engineering, construction engineering, physics, chemistry, medical diagnostics, agriculture and dairy.
| Author | : Mark E. Orazem |
| Publisher | : John Wiley & Sons |
| Total Pages | : 763 |
| Release | : 2017-04-24 |
| Genre | : Science |
| ISBN | : 1118527399 |
Provides fundamentals needed to apply impedance spectroscopy to a broad range of applications with emphasis on obtaining physically meaningful insights from measurements. Emphasizes fundamentals applicable to a broad range of applications including corrosion, biomedical devices, semiconductors, batteries, fuel cells, coatings, analytical chemistry, electrocatalysis, materials, and sensors Provides illustrative examples throughout the text that show how the principles are applied to common impedance problems New Edition has improved pedagogy, with more than twice the number of examples New Edition has more in-depth treatment of background material needed to understand impedance spectroscopy, including electrochemistry, complex variables, and differential equations New Edition includes expanded treatment of the influence of mass transport and kinetics and reflects recent advances in understanding frequency dispersion and constant-phase elements
| Author | : J. Ross Macdonald |
| Publisher | : Wiley-Interscience |
| Total Pages | : 368 |
| Release | : 1987-06-23 |
| Genre | : Science |
| ISBN | : 9780471831228 |
This is the first book-length, integrated treatment of impedance spectroscopy with an emphasis on solid state electrochemical systems. Impedance spectroscopy is a method for characterizing the electrical behavior of systems in which the overall system behavior is determined by a number of coupled processes, each proceeding at a different rate. The scope of this volume is comprehensive: provides coverage of fundamental theory, illustrates applications of the technique, and discusses practical considerations in regard to data acquisition and analysis. Those with little prior experience in impedance measurements will find this an excellent introduction. Senior investigators will find that the book provides a useful summary of fundamentals as well as a survey of recent developments in the field.
